ObjectiveTo assess the setting time (ST), flow (FL), radiopacity (RD), solubility (SB) and
dimensional change following setting (DC) of different sealers (AH
Plus®, Polifil, Apexit Plus®, Sealapex®,
Endométhasone® and Endofill® according to American
National Standards Institute/American Dental Association (ANSI/ADA) Specification
57. Material and methodsFive samples of each material were used for each test. For ST, cast rings were
filled with sealers and tested with a Gilmore needle. For FL, the sealer was
placed on a glass plate. After 180 s, another plate with 20 g and a load of 100 g
were applied on the material, and the diameters of the discs formed were measured.
In RD, circular molds were filled with the sealers, radiographed and analyzed
using Digora software. For SB, circular molds were filled with the sealers, a
nylon thread was placed inside the material and another glass plate was positioned
on the set, pressed and stored at 37ºC. Samples were weighed, placed in water,
dried and reweighed. The water used for SB was analyzed by atomic absorption
spectrometry. For DC, circular molds were filled with the sealers, covered by
glass plates and stored at 37ºC. Samples were measured and stored in water for 30
days. After this period, they were dryed and measured again. ResultsRegarding ST, AH Plus®, Apexit® and Endofil®
sealers are in accordance with ANSI/ADA standards. Endométhasone's manufacturer
did not mention the ST; Polifil is an experimental sealer and Sealapex®
did not set. Considering RD, SB and DC, all sealers were in accordance with
ANSI/ADA. The spectrometric analysis showed that a significant amount of
K+ and Zn2+ ions was released from Apexit
Plus® and Endofill®, respectively. ConclusionExcept for DC, all other physicochemical properties of the tested sealers
conformed to ANSI/ADA requirements.