SHI, Min(hk%>Optically active a-symmetric ( 1 , 2 : 4, S)-diepoxypentane equivdent ( 10 has been synthesized in eight steps with moderate yields and diastereomeric excess by using Sharpless asymmetric dihydroxylation (AD reaction). Compound 10 can be used to prepare SYII 1,3401 subunit h mhval produet.'Dedicated to Professor ZHOU Wei-Shan on the occasion of his 80th birthday.
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