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A facile strategy is proposed to construct a highly active oxidation catalyst with optimally distributed titanium coordination states containing "TiO4" and "TiO6" species. The "TiO6" species in TS-1(+) shows a superior catalytic oxidation activity, which is 2-3 times that of "TiO4" species in TS-1.

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The Lewis acidity of titanosilicates determines oxime selectivity in ammoximation by influencing the reaction activation energy of Ti–OOH for the highly efficient formation of NH2OH.

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