Experimental investigation on the influence of load interaction on the life of Single Crystal Nickel-based Superalloy is conducted. Three kinds of load spectrums considering single and coupled failure mode are designed. Life tests are carried out under creep, thermo-mechanical fatigue (TMF), and creep-TMF interaction loading. The test results show that test lives, under the creep-TMF interaction loading, are lower than the life predictions given by the linear damage accumulation (LDA) rule, indicating that the load coupling can accelerate the damage evolution process. The microstructure of fractured specimens shows that under the creep-TMF interaction loading, rafting cause more dislocations to accumulate in the at γ/γ′ phase boundary, which could be the evidence of life decrease.
This paper presents a total nitrogen (TN) detection system based on electrochemical measurement. This system integrates a three-electrode system and a specially designed detection circuit. The dynamic response characteristic of the three-electrode system during TN electrochemical determination process was studied. The equivalent circuit of the three-electrode system was used to analyze factors of interference and signal instability. Through theoretical derivations and experimental proof, a time-domain model of signal response was established and two main factors, electric double layer capacitor and holding time, were put forward. Smooth and steady signal was achieved by optimizing these two main factors. Water sample of Taihu Lake was detected by this developed TN detection system with acceptable accuracy.
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