In order to improve the anti-oxidation of C/C composites, a C/SiC functionally graded coating for C/C composites was prepared by low pressure chemical vapor deposition (LPCVD) using methyltrichlorosilane (MTS, CH3SiCl3) and H2 as precursors. The relative amount of C and SiC in coatings was varied by controlling the input ratio of H2 to MTS. The phase composition and morphology were examined by scanning electron microscope (SEM) and X-ray diffraction (XRD), and the content distribution of C and SiC phases were investigated by energy dispersive spectroscopy (EDS). The isothermal oxidation test was evaluated at 900 °C and 1500 °C respectively. The results showed that the as-obtained coatings were possessed of a dense and uniform structure, and the SiC content in coatings increased with an increment of the molar ratio of H2 to MTS. The C/SiC coating had a good oxidation resistance.
In order to further study the cracks initiation and distribution mechanism of SiC coating, then optimize the coating structure and composition on surface of C/C composites, CVD method is used to deposit SiC coating on C/C composites and pyrolytic carbon. Through the analysis on the reasons of cracks initiation via SEM, the influence of different kinds of substrates and the toughening of SiC whisker on the cracks initiation and distribution are researched. The results show that the cracks easily form in the area near the defects and sample edge, and the cracks also mainly distribute in the direction which are perpendicular to the first fiber layer. Compared with pyrolytic carbon matrix, cracks on C/C composites matrix are width and numerous, and SiC whisker toughening coating can significantly reduce the number of cracks.
Resin lenses have substituted for glass lenses to be dominant productions in eyeglasses market
because of lightweight, anti-impaction and easy molding. However, the problem existed that the wear
resistance of resin lenses was inferior. In order to increase the wear resistance of resin lenses, we coated
DLC film on PC by the method of RF-PCVD, researched the influence of depositing power, gas
concentration, time on the performance of coating, chose the optimum technological parameters. The
component of coating was testified by XPS. The hardness and wear resistance were tested. The results
showed that DLC films deposited on PC could improve the wear resistance of material.
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