All of the parameters (ethanol concentration, extraction time and extraction temperature) used in this research have the significant effect on the extraction efficiency of total phenolic content in rosehip extracts (P < 0.05). The solvent concentration was proved to be the most significant effective on the yields obtained by ultrasound-assisted extraction.
Naproxen is one of the mostly used drugs worldwide and is most abundant in wastewater. This study aims to adsorb naproxen from wastewater using magnetically modified carbon-based adsorbents. These adsorbents have very large specific area for naproxen adsorption, and magnetite modification provides easy separation and regeneration. The co-precipitation method was used for magnetic modification. Adsorption process was carried out in batches. The effect of adsorption variables was investigated. Langmuir, Freundlich, and Dubinin-Radushkevich isotherms were applied to the equilibrium data. The maximum adsorption capacities of adsorbents from Langmuir isotherm were found as 20.75 mg/g for magnetic multiwall carbon nanotubes and 87.79 mg/g for magnetic activated carbon. Pseudo-first-order kinetic model, pseudosecond-order kinetic model, intra-particle diffusion model, and Bangham model were used for determination of adsorption mechanisms. The rate-limiting step is electron exchange between the adsorbent and adsorbate. Both film diffusion and intra-particle diffusion occur while the adsorption process. DG°, DS°, and DH°were calculated for the process.
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