Magnesium oxide nanoparticles (MgO NPs) were synthesized by a green method using the peels of Persimmon extract as the reducing agent , magnesium nitrate, and NaOH. This method is eco-friendly and non-toxic. In this study, an ultrasound device was used to reduce the particle size, with the impact on the energy gap was set at the beginning at 5.39 eV and then turned to 4.10 eV. The morphological analysis using atomic force microscopy (AFM) showed that the grain size for MgO NPs was 67.70 nm which became 42.33 nm after the use of the ultrasound. The shape of the particles was almost spherical and became cylindrical. In addition the Field-Emission Scanning Electron Microscopy (FESEM) analysis showed that the average particle size was reduced and the spherical shape was changed into cylindrical flakes. The antibacterial activity of MgO Nps was measured against both gram positive and negative bacteria (Staphylococcus aureus and Escherichia coli, respectively) for both the synthesized and the scaled-down particles by the ultrasonic. MgO NPs showed an efficacy at a minimum inhibitory concentration (MIC) of 500 μg/ml, with the better effect being observed after the ultrasonic treatment of the MgO NPs.
Copper oxide nanoparticles (CuO NPs) were synthesized by two methods. The first was chemical method by using copper nitrate Cu (NO3)2 and NaOH, while the second was green method by using Eucalyptus camaldulensis leaves extract and Cu (NO3)2. These methods easily give a large scale production of CuO nanoparticles. X-ray diffraction pattern (XRD) reveals single phase monoclinic structure. The average crystalline size of CuO NPs was measured and used by Scherrer equation which found 44.06nm from chemical method, while the average crystalline size was found from green method was 27.2nm. The morphology analysis using atomic force microscopy showed that the grain size for CuO NPs was synthesized by chemical and green methods were 77.70 and 89.24 nm, respectively. The effectiveness of copper oxide nanoparticles on bacteria was measured for both gram positive, negative and fungi, copper oxide minutes showed excellent efficacy on biofilm formation.
In this study, zinc oxide was prepared by pulsed laser ablation method (PLAL), which is an easy-to-use and inexpensive physical method. The optical properties were studied using UV-Vis spectrometers, structure properties by (XRD) to calculate the crystalline size, and particle size determination by Field emission scanning electron microscopy (FE-SEM) and (EDS), transmission electron microscopy (TEM) assays and it was proved that they are within the ideal nanoscale for biological application. These ZnO NPs were employed on the inhibitory activity of different types of Gram-positive and Gram-negative bacteria, as well as on fungi, and it was noted their ability to penetrate the bacterial cell wall and inhibit its action.
Nanostructured indium doped CdO thin films were prepared by spray pyrolysis on glass substrate and annealed at 200-400 ᵒC for 1 hour. The structural, optical, and electrical properties of prepared films were studied using different techniques such as optical transmission, photoluminescence, X-ray diffraction, and Hall measurement. X-ray analysis shows that the In doped CdO films are preferentially orientated along (111) crystallographic directions. Increasing of annealing temperature increases the films packing density and reorient the crystallites along (1 1 1) plane. The optical transmissions of all annealed films decreased with increasing annealing temperature. An increasing in the absorbance and photoluminescence spectra with increasing annealing temperature was denoted in all films. The band gap value of CdO:4%In equals to 2.5 eV and it decreases with annealing temperature and reaches of 2.45 eV for 400°C. The resistivity of annealed films decreased as annealing temperature increased. While high conductivity achieved in the present study is found to be 11.37 ×102 (Ω.cm)-1 for annealing at 400°C.
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