The thermal conductivities and the strengths of fumed silica-based thermal insulations prepared by the dry process and the resin infiltration method have been studied. Infiltration of the insulation samples prepared by dry processing of mixtures, consisting of fumed silica, ceramic fiber and a SiC opacifier, was performed to strengthen their binding structure. The high temperature thermal conductivities for the insulation samples obtained by the resin infiltration method were similar to those for the samples prepared by the dry process. On the other hand, the bending strengths for the former were superior to those for the latter. However, the resin-infiltrated samples were more brittle than the samples obtained by the dry process due to the occurrence of rigid bonding between the fibers and the infiltrated resin in the porous insulations. The thermosetting resin solution infiltration method appeared to be applicable to producing a dust-free fumed silica-based thermal insulation.
Microporous thermal insulations were prepared from mixtures of nano-sized fumed silica, micron-sized fibers and opacifier particles. Those micron-sized particles were dry coated with nano-sized fumed silica particles by mechanical process using a compressive-shear type mill. The effect of nanoparticle coating on the thermal conductivity of the insulation media was investigated using a hot-wire method. Effect of nanoparticle coating was found to be more pronounced for the insulation composed of fumed silica and fiber than for the one composed of fumed silica, fiber and an opacifier. By adding 15% SiC or TiO2 opacifier, the thermal conductivity of the insulation samples could be lowered to 0.08 Wm(-1) K(-1) at temperature range of 805 approximately 817 degrees C. The temperature dependent thermal conductivity of the sample containing glass fiber did not exhibit any remarkable changes compared to the one containing ceramic fiber.
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