Through flotation recovery of Silver (Ag) from Zinc acid-leaching residue (ZALR) was investigated in this study. The study adopted the single factor and orthogonal test reveal interactions among all considerable influence factors including sodium sulphide (SS) as regulator, ammonium butyl dithiophosphate (ABD) as major collector, GC as minor collector, interaction between ABD and GC, OC as flotation carrier, and pulp density. The experimental results show the flotation of the circuit composited of one rougher, one cleaner, one scavenger and middlings being back to the next rough flotation together is practical way and that the concentrate containing Ag 10890.0g/t, recovery77.43% can be obtained from the residue (Ag grade 340g/t). The optimum roughing flotation process is: the pH value of flotation pulp is 3.0~4.0, the pulp density is about 45wt.%, ABD dosage is 900g/t, GC dosage is 50g/t, OC dosage is 2000g/t, and BK201 dosage is 100g/t.
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