Static and dynamic experiments were used to evaluate scale inhibition performance of polyaspartic acid derivative (PASP-SEA-ASP). The static experiments showed that the PASP-SEA-ASP had good scale inhibition performance and the scale inhibition rate exceeded 80% when the PASP-SEA-ASP was 2 mg•L-1 and the solution temperature was 40 OC. In the dynamic experiments, almost no scale formed on the heat transfer surface and the fouling thermal resistance decreases extraordinarily with PASP-SEA-ASP treatment experiment compared with the experiment without treatment. The PASP-SEA-ASP could be used in industrial cooling water systems.
Static and dynamic experiments were used to evaluate scale inhibition performance of modified polyaspartic acid (PASP-ASP). The static experiments showed that the PASP-ASP had good scale inhibition performance and the scale inhibition rate exceeded 98% when the PASP-ASP was 2 mg·L-1 and the solution temperature was 40 OC. In the dynamic experiments, almost no scale was formed on the heat transfer surface and the fouling thermal resistance decreases extraordinarily with PASP-ASP treatment experiment compared with the experiment without treatment. The PASP-ASP could be used in industrial cooling water systems.
Cross-linked carboxymethyl starch CMS was synthesized with cross-linked starch as raw material, sodium chloroacetate as etherification agent and sodium hydroxide as catalyst, and the structure of the product was characterized by FTIR, SEM and XRD. The optimum synthesis conditions of CMS were m (CSt): m (MCA) = 5:3, NaOH dosage 12 ml, reaction temperature 55 °C and reaction time 3 h. When the concentration of copper ion in the simulated water sample was 25 mg/L and the dosage of CMS was 2 g/L, the removal rate of copper ion was 96.0%, and the adsorption capacity of CMS was 15.4 mg/g.
The polyaspartic acid derivative compound was applicated in circulating cooling water system with high concentration multiple with the water quality of circulating cooling water system was characterized by higher hardness, higher alkalinity and higher corrosive ion content in order to solve the problem of scale and corrosion of the circulating cooling water system. The formulation of the polyaspartic acid derivative compound was determined to be PASP-AESA-ASP, ZnSO4, HPAA and BTA with the mass ratio of 15:4:6:0.1. The polyaspartic acid derivative compound had a good protective effect on A3 carbon steel in high-concentration-salt water and good biodegradability.
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