The analysis of chemical species is one of the most fundamental and long-standing challenges in fiber-optic sensors research. Existing sensor architectures require a spatial overlap between light and the substance being tested and rely either on structural modifications of standard fibers or on specialty photonic crystal fibers. In this work, we report an optomechanical fiber sensor that addresses liquids outside the cladding of standard, 8/125 μm single-mode fibers with no structural intervention. Measurements are based on forward stimulated Brillouin scattering by radial, guided acoustic modes of the fiber structure. The acoustic modes are stimulated by an optical pump pulse and probed by an optical signal wave, both confined to the core. The acoustic vibrations induce a nonreciprocal phase delay to the signal wave, which is monitored in a Sagnac interferometer loop configuration. The measured resonance frequencies and excitation strengths of individual modes agree with the predictions of a corresponding quantitative analysis. The acoustic reflectivity at the outer cladding boundary and the acoustic impedance of the surrounding medium are extracted from cavity lifetime measurements of multiple modes. The acoustic impedances of deionized water and ethanol are measured with better than 1% accuracy. The measurements successfully distinguish between aqueous solutions with 0, 4%, 8%, and 12% concentrations of dissolved salt. The new fiber-sensing paradigm might be used in the monitoring of industrial processes involving ionic solutions.

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Optical fibres constitute an exceptional sensing platform. However, standard fibres present an inherent sensing challenge: they confine light to an inner core. Consequently, distributed fibre sensors are restricted to the measurement of conditions that prevail within the core. This work presents distributed analysis of media outside unmodified, standard fibre. Measurements are based on stimulated scattering by guided acoustic modes, which allow us to listen where we cannot look. The protocol overcomes a major difficulty: guided acoustic waves induce forward scattering, which cannot be mapped using time-of-flight. The solution relies on mapping the Rayleigh backscatter contributions of two optical tones, which are coupled by the acoustic wave. Analysis is demonstrated over 3 km of fibre with 100 m resolution. Measurements distinguish between air, ethanol and water outside the cladding, and between air and water outside polyimide-coated fibres. The results establish a new sensor configuration: optomechanical time-domain reflectometry, with several potential applications.

A new technique for Brillouin scattering-based, distributed fiber-optic measurements of temperature and strain is proposed, analyzed, simulated, and demonstrated. Broadband Brillouin pump and signal waves are drawn from the filtered amplified spontaneous emission of an erbium-doped fiber amplifier, providing high spatial resolution. The reconstruction of the position-dependent Brillouin gain spectra along 5 cm of a silica single-mode fiber under test, with a spatial resolution of 4 mm, is experimentally demonstrated using a 25 GHz-wide amplified spontaneous emission source. A 4 mm-long localized hot spot is identified by the measurements. The uncertainty in the reconstruction of the local Brillouin frequency shift is ± 1.5 MHz. The single correlation peak between the pump and signal is scanned along a fiber under test using a mechanical variable delay line. The analysis of the expected spatial resolution and the measurement signal-to-noise ratio is provided. The measurement principle is supported by numerical simulations of the stimulated acoustic field as a function of position and time. Unlike most other Brillouin optical correlation domain analysis configurations, the proposed scheme is not restricted by the bandwidth of available electro-optic modulators, microwave synthesizers, or pattern generators. Resolution is scalable to less than one millimeter in highly nonlinear media.

The analysis of surrounding media has been a long-standing challenge of optical fiber sensors. Measurements are difficult due to the confinement of light to the inner core of standard fibers. Over the last two years, new sensor concepts have enabled the analysis of liquids outside the cladding boundary, where light does not reach. Sensing is based on opto-mechanical, forward stimulated Brillouin scattering (F-SBS) interactions between guided light and sound waves. In most previous studies, however, the protective polymer coating of the fiber had to be removed first. In this work, we report the opto-mechanical analysis of liquids outside commercially available, standard single-mode fibers with polyimide coating. The polyimide layer provides mechanical protection but can also transmit acoustic waves from the fiber cladding toward outside media. The comprehensive analysis of opto-mechanical coupling in coated fibers that are immersed in liquid is provided. The model shows that F-SBS spectra in coated fibers are more complex than those of bare fibers and strongly depend on the exact coating diameter and the choice of acoustic mode. Nevertheless, sensing outside coated fibers is demonstrated experimentally. Integrated measurements over 100 m of fiber clearly distinguish between air, ethanol, and water outside polyimide coating. Measured spectra are in close quantitative agreement with the analytic predictions. Furthermore, distributed opto-mechanical time-domain reflectometry mapping of water and ethanol outside coated fiber is reported, with a spatial resolution of 100 m. The results represent a large step toward practical opto-mechanical fiber sensors.

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The proper function of protective coating layers is essential for the handling and application of brittle optical fibers. The elastic parameters of polymer coatings can be studied through off-line analysis of test samples. However, the monitoring of these properties on a working fiber during service is challenging. In this work, we use forward stimulated Brillouin scattering processes in standard single mode fibers to measure the acoustic velocity in several types of coating layers. Pump light launches short acoustic pulses outward from the core of the fiber. Multiple reflections at the boundaries between cladding and coating, and between coating and air, form a series of delayed acoustic echoes across the core. These echoes are monitored, in turn, by photo-elastic phase modulation of probe light. Data are collected at temperatures between 25-120 °C. The thermal dependence of the acoustic velocities in several coatings and of the F-SBS resonance frequencies is investigated. Observations are corroborated by calculations. The proposed technique is well suited for research and development of coating materials, production line quality control, reliability studies and preventive maintenance of working fibers.

A new, hybrid time-domain and correlation-domain Brillouin analysis technique is proposed and demonstrated, providing a large number of high-resolution acquisition points. The method is based on dual-layer hierarchal encoding of both amplitude and phase. The pump and signal waves are co-modulated by a relatively short, high-rate binary phase sequence. The phase modulation introduces Brillouin interactions in a large number of discrete and localized correlation peaks along the fiber under test. In addition, the pump wave is also amplitude-modulated by a slower, carefully synthesized, long on-off-keying sequence. Brillouin interactions at the correlation peaks imprint weak replicas of the pump amplitude sequence on the intensity of the output signal wave. The Brillouin amplifications at individual correlation peaks are resolved by radar-like, matched-filter processing of the output signal, following a recently-proposed incoherent compression protocol. The method provides two significant advantages with respect to previous, pulse-gated correlation-domain analysis schemes, which involved a single pump pulse. First, compression of the extended pulse sequence enhances the measurement signal-to-noise ratio, which is equivalent to that of a large number of averages over repeating single-pulse acquisitions. The acquisition times are potentially much reduced, and the number of resolution points that may be practically interrogated increases accordingly. Second, the peak power level of the pump pulses may be lowered. Hence, the onset of phase pattern distortion due to self-phase modulation is deferred, and the measurement range can be increased. Using the proposed method, the acquisition of Brillouin gain spectra over a 2.2 km-long fiber with a spatial resolution of 2 cm is demonstrated experimentally. The entire set of 110,000 resolution points is interrogated using only 499 position scans per choice of frequency offset between pump and signal. A 5 cm-long hot-spot, located towards the output end of the pump wave, is properly recognized in the measurements.