The preparation and application of ultra-clean coal is one of the important aspects of clean energy technology. However, the preparation of ultra-clean coal is mainly chemical methods, which are low in efficiency, high in energy consumption and expensive. It is urgent to find an effective method to prepare ultra-clean coal. In this paper, the combined method of grinding and the collector gasification flotation method was used to obtain ultra-clean coal. The effects of grinding time on the particle size composition, mineral dissociation, surface properties and flotation results of coal samples were studied. The grinding test results show that with the increase in grinding time, the particle size and the pore diameter of coal samples decreased gradually, while the specific surface area and pore volume of coal samples gradually increased. When the grinding time was 20 min, the D90 and D[4,3] of grinding products were 5.20 um and 4.23 um, respectively. The ash content of −1.3 g/cm3 was less than 1% when the grinding time was 20 min. Compared with the traditional flotation method, the collector gasification flotation method can obtain a higher concentrate yield and lower concentrate ash content. When the amount of collector was 2.0 kg/t, the yield of clean coal obtained by the collector gasification flotation method was 4.1% higher than that by the traditional flotation method, while the ash content of clean coal was 0.3% lower.
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