The fabrication of periodic nanostructures with a fine control of their dimensions is performed on poly(methyl methacrylate) (PMMA) thin films using an atomic force microscope technique called dynamic plowing lithography (DPL). Different scratching directions are investigated first when generating single grooves with DPL. In particular, the depth, the width and the periodicity of the machined grooves as well the height of the pileup , formed on the side of the grooves, are assessed. It was found that these features are not significantly affected by the scratching direction, except when processing took place in a direction away from the cantilever probe and parallel to its main axis. For a given scratching direction, arrays of regular grooves are then obtained by controlling the feed, i.e. the distance between two machining lines. A scan-scratch tip trace is also used to reduce processing time and tip wear. However, irregular patterns are created when combining two layers oriented at different angles and where each layer defines an array of grooves. Thus, a "combination writing" method was implemented to fabricate arrays of grooves with a well-defined wavelength of 30 nm, which was twice the feed value utilized. Checkerboard, diamond-shaped, and hexagonal nanodots were also fabricated. These were obtained by using the combination writing method and 2 by varying the orientation and the number of layers. The density of the nanodots achieved could be as high as 1.9×10 9 nanodots per mm 2 .

Aluminium-based composites are increasingly applied within the aerospace and automotive industries. Tribological phenomena such as friction and wear, however, negatively affect the reliability of devices that include moving parts; the mechanisms of friction and wear are particularly unclear at the nanoscale. In the present work, pin-on-disc wear testing and atomic force microscopy nanoscratching were performed to investigate the macro and nanoscale wear behaviour of an Al-Al 2 O 3 nanocomposite fabricated using selective laser melting. The experimental results indicate that the Al 2 O 3 reinforcement contributed to the macroscale wear-behaviour enhancement for composites with smaller wear rates compared to pure Al. Irregular pore surfaces were found to result in dramatic fluctuations in the frictional coefficient at the pore position within the nanoscratching. Both the size effect and the workingprinciple difference contributed to the difference in frictional coefficients at both the macroscale and the nanoscale.

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