Disc coal samples with different water content were tested using the split Hopkinson press bar test system. Their dynamic tensile failure process was monitored via an ultra-high-speed digital image correlation system. The deformation trend and failure characteristics as a function of the water content were analyzed, and the water content effect on dynamic mechanical properties was investigated. The results demonstrated that the dynamic stress–strain curve of the coal samples consisted of four stages. As the water content increased, the coal sample brittleness degraded, while its ductility was enhanced. Quadratic polynomial functions can describe dynamic peak stress, peak strain, and loading pressure. Under different loading pressures, the dynamic peak stress exhibited a concave bending trend as the water content increased. The coal sample's dynamic tensile strength had a strong rate correlation, and the saturated coal sample exhibited the highest rate correlation. Under high-rate loading, the inertia effect and the Stefan effect of water in coal samples hinder the initiation and propagation of coal sample cracks, improving the coal sample's strength. The research results provide a basic theoretical basis for the prevention and control of rock burst in coal mines.
Backfill mining has become an important part of coal mine green mining technology. In this paper, the spatiotemporal characteristics of coupling effect between the roof and dense backfill body were analyzed by theoretical analysis and similar simulation test, and Xingtai Mine in China was taken as an engineering case for verification. The results show that the larger subsidence of the roof is, the stronger the supporting capacity of the backfill body is, and the interaction between the two is more obvious, thus showing a coupling effect. This coupling effect presents a regular variation with the increase of backfill distance and time, that is, the coupling degree of roof and backfill body is high in the middle of goaf and low in the vicinity of the coal pillar in spatial distribution, and the coupling behavior of roof and backfill body continues to occur slowly with time. Through the monitoring of stress and displacement in the engineering site and the analysis of borehole observation results, the spatiotemporal coupling effect between roof subsidence and backfill support is fully verified. The research results are of great significance to the control of surrounding rock in backfill mining, the study of the mechanical aging characteristics of backfilling materials, and the optimization of backfill body support performance.
To explore the strength development characteristics and engineering performance of different coal-based solid waste filling materials cemented into filling body, coal gangue was used as coarse material, fly ash, desulfurization gypsum, gasification slag, and furnace bottom slag as fine material, and cement as a gelling agent. The uniaxial compressive strength (UCS) and bleeding rate of coal-based solid waste cemented backfill (CBSWCB) were tested by an orthogonal experiment, and the influencing factors of mechanical properties and strength development were analyzed. The multiple generalized linear model of strength and bleeding rate was established, and the optimal filling material ratio was determined. The engineering performance index of CBSWCB with the optimal ratio was tested. The results show the following points: (1) the concentration and content of desulfurization gypsum had a great influence on the early compressive strength of CBSWCB, while fly ash, gasification slag, and furnace bottom slag had little influence on the early compressive strength. (2) High concentration, high content of fly ash and furnace bottom slag, low content of desulfurization gypsum, and gasification slag can significantly improve the early strength. High concentration and high content of fly ash, low content of gasification slag, furnace bottom slag, and desulfurization gypsum are beneficial to the later strength increase. (3) Under the optimal ratio scheme, the bleeding rate of CBSWCB was 1.6%, the slump was 16.6 cm, the cohesion was general, the segregation resistance was good, the initial setting time was 5.42 h, the final setting time was 7 h, and the early strength after curing for 8 h reached 0.24 MPa.
Microwave pyrolysis is a new research method for deeply processing of low-rank coal. On basis of experiments, this paper conducted comparative study on microwave co-pyrolysis products of low-rank coal under circulating gas (CG) and N 2 atmosphere, respectively. The composition and content of tar and bluecoke were analyzed by gas chromatography-mass spectrometry and fourier transform infrared spectrometer. The results indicated that compared with N 2 atmosphere, the yield of liquid products (tar and pyrolysis water) obtained under CG atmosphere was higher than 8.0 wt.%, whereas the bluecoke yield was lower than 4.4 wt.%; The content of S element in the bluecoke obtained under CG atmosphere was 0.16 wt.% to meet Bluecoke Standard S-1 Grade, and the N element content was just 0.67 wt.%. Furthermore, the content of -OH、C=C and -C=O functional groups in the bluecoke were higher; The alkanes compounds content in tar obtained under CG atmosphere was 8.10 wt.% higher than that under N 2 atmosphere, meanwhile, the aromatic hydrocarbons compounds content was 37.4 wt.% lower than that under N 2 atmosphere.
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