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Nannocystins are a family of 21-membered cyclodepsipeptides with excellent anticancer activity. Yet their macrocyclic architecture poses a significant challenge to structure modification. Herein this issue has been addressed by leveraging...

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A new enantiopure 6-monobromo-substituted BINAP has been prepared via a one-step nickel-catalyzed coupling reaction in moderate yield. It is an important intermediate for asymmetric 2,2 0 -bis(diphenylphosphino)-1,1 0 -binaphthyl (BINAP) derivatives. Its structure was elucidated by NMR spectral and elemental analysis.