Experiments were carried out with different apparatus to compact electrolytic copper powders at distinct loading speeds. It appears that green densities of compacts prepared by HVC out-number that by conventional compaction by one percent. Compacts by quasistatic compaction are almost as dense as those by HVC under comparable peak pressure. The relationship between green compact density and peak pressure accords with Hang Pei-yun formula well. Spring-backs of HVC compacts are far smaller than those of conventional compaction and quasi-static compaction. HVC compacts are harder than compacts by conventional compaction and quasi-static compaction when they have the same density.
Four different super-black conversion films on ZK61M magnesium alloys were investigated in this work. Macro-and micro-morphologies of the conversion films were observed using a digital camera and scanning electron microscope, respectively. Salt spray testing and electrochemical measurements were used to examine the corrosion resistance of the conversion films. The emissivities of the conversion films were measured using the Fourier transform infrared spectrometry. The results show that all conversion films reduced the corrosion rate of the magnesium alloy substrates effectively; in particular, the film prepared using 230 g L −1 HF + 150 g L −1 Na 2 Cr 2 O 7 •2H 2 O + 2.5 g L −1 CaF 2 mixed solution had a higher corrosion resistance. Moreover, the emissivities of the conversion films prepared using 230
This present work investigates the effects of sintering temperature on densification, mechanical properties and microstructure of Al-based alloy pressed by high-velocity compaction. The green samples were heated under the flow of high pure (99.99 wt%) N2. The heating rate was 4 °C/min before 315 °C. For reducing the residual stress, the samples were isothermally held for one h. Then, the specimens were respectively heated at the rate of 10 °C/min to the temperature between 540 °C and 700 °C, held for one h, and then furnace-cooled to the room temperature. Results indicate that when the sintered temperature was 640 °C, both the sintered density and mechanical properties was optimum. Differential Scanning Calorimetry, X-ray diffraction of sintered samples, Scanning Electron Microscopy, Energy Dispersive Spectroscopy, and Transmission Electron Microscope were used to analyse the microstructure and phases.
In this research, the effects of the compaction velocity on the sinterability of the Al–Fe–Cr–Ti powder metallurgy (PM) alloy by high velocity compaction were investigated. The Al–Fe–Cr–Ti alloy powder was compacted with different velocities by high velocity compaction and then sintered under a flow of high pure (99.999 wt%) nitrogen gas. Results indicated that both the sintered density and mechanical properties increased with increasing compaction velocity. By increasing the compaction velocity, the shrinkage of the sintered samples decreased. A maximum sintered density of 2.85 gcm−3 (relative density is 98%) was obtained when the compaction velocity was 9.4 ms−1. The radial and axial shrinkage were controlled to less than 1% at a compaction velocity of 9.4 ms−1. At a compaction velocity of 9.4 ms−1, sintered compacts with an ultimate tensile strength of 222 MPa and a yield strength of 160 MPa were achieved. The maximum elongation was observed to be 2.6%. The enhanced tensile properties of the Al–Fe–Cr–Ti alloy were mainly due to particle boundary strengthening.
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