Nd3+, Y3+: SrF2 transparent ceramics were successfully synthesized by two methods: hot-forming and hot-pressing techniques. The mechanical properties and optical properties of the hot-formed Nd3+, Y3+: SrF2 transparent ceramics were much better than that of single crystal. On the other hand, the transmittance of the hot-formed transparent ceramics with different deformation rate reached up to 90% at 1054 nm, which is superior to the hot-pressed ceramics. Furthermore, the fracture toughness of hot-formed Nd3+, Y3+: SrF2 transparent ceramics with the deformation rate of 51% reached up to 0.70 MPa m1/2, which is nearly 1.5 times higher than that of as-grown single crystal. The full width at half maximum (FWHM) of the hot-formed ceramic is larger than that of the single crystal at 1053 nm under continuous-wave (CW) laser operation. The thermal conductivity of Nd3+, Y3+: SrF2 single crystal and hot-formed ceramics were also discussed.
Compressive creep behavior of a Mg-Al alloy containing a small amount of Nd and Gd (Mg-6Al-1Nd-1.5Gd) was investigated at temperatures from 150 °C to 200 °C under a constant applied stress of 90 MPa, and its microstructure before and after creep testing was compared. Results showed that steady-state creep rate of the alloy was only 1.946 × 10−8 /s at 150 °C, and was increased by four times and almost one order of magnitude at 175 °C and 200 °C, respectively. The microstructure of the alloy mainly consists of α-Mg, β-Mg17Al12 phases, and Al2RE phases, which were distributed both in dendrites of α-Mg and at grain boundaries originally. After creep for 120 h, more Al2RE phases were aggregated at grain boundaries. The continuous β-Mg17Al12 phase turned into dispersed dot-like or blocky particles. As the test temperature increased, the number of dislocation lines gradually increased due to the increase of creep strain. Meanwhile, dislocation tangle and dislocation pile-ups occurred near grain boundaries. However, obvious slip traces and slip lines appeared inside α-Mg dendrites at 175 °C and 200 °C, respectively, indicating that 〈c + a〉 non-basal slip system was activated, creep resistance decreased dramatically.
TiB2/Mg-4Al-1.5Si magnesium matrix composites were prepared by semi-solid stirring assisted ultrasonic treatment, the primary Mg2Si phases in the composites exhibit polygon with sharp corners, and the eutectic Mg2Si phases appear thin Chinese-script or short-strip shape. To reduce stress concentration around the sharp corners (tips) of the Mg2Si phases, the morphology of the Mg2Si phases was further modified by solution treatment at 420 °C for 24 h, and the effects of the morphology modification of the Mg2Si phases on the mechanical properties of the composites were investigated. The results showed that after the solution treatment, the sharp corners of the primary Mg2Si phases were blunted, and the partial branches of the eutectic Mg2Si phases were dissolved into particles. The Vickers-hardness, ultimate tensile strength, yield strength, and elongation of the composites were increased by 11.50%, 33.28%, 28.57%, and 27.17% compared with those of unmodified composites, respectively. The solution treatment exhibits a more significant strengthening effect for the composites in hardness, ultimate tensile strength, and yield strength compared with the matrix alloys.
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