A nondestructive technique is described for the measurement of elastic constants of isotropic plates using ultrasonic Rayleigh-Lamb waves. The experimental method employs continuous harmonic waves and a pair of variable-angle contact transducers in pitch-catch mode. The phase velocity of the R-L waves at a particular frequency is determined from the phase shift over a measured path length. This simple experimental technique can measure phase velocity over the range 1-10 m m / p with an error of less than 0.5% over a frequency range of 50 kHz-2 MHz. Individual symmetric and antisymmetric modes can be generated through the selection of transducer angle and frequency. Young's modulus and Poisson's ratio for the material are calculated from measurements of frequency and phase velocity by a nonlinear least squares solution to the dispersion equations. The sensitivity of the nonlinear least squares function to the measurement region of the dispersion curve is investigated. It was found that estimations of material properties are more accurate and less sensitive to small experimental errors when only selected frequencies and R-L modes are used in the least squares calculation. This technique is demonstrated with several isotropic materials and with both thick (6 mm) and thin (0.8 mm) plates. Values for elastic constants determined by the contact transducer Lamb wave technique compare favorably with values measured using the pulse-echo-overlap method. The uncertainty in measurements of Young's modulus and Poisson's ratio was less than 1% and 2%, respectively. The technique has advantages over more traditional methods for measuring elastic properties when it is desirable to use wavelengths greater than the plate thickness, when properties may vary with frequency, or when it is necessary to measure in-plane elastic properties of thin plate structures.
Transformation plasticity in magnesia-partially-stabilized zirconia (Mg-PSZ) is studied using a split Hopkinson pressure bar modified for ceramic materials.. Axial and transverse strains are measured under uniaxial compressive loading at a strain rate of 250/s. The transformation yield stress is found to increase from 900 MPa under quasi-static loading to 1.2 GPa at high strain rate. Post-yield deformation is characterized by shear and volumetric plastic strains up to 1.2%. During unloading, the axial and transverse plastic strains are partially recovered while the volume is conserved. Axially oriented microcracks are observed but they do no contribute significantly to plastic deformation in Mg-PSZ. [
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