Sensitive new analytical methods for water-soluble aliphatic aldehydes has been introduced. Versatile spot plate, paper, silica gel, and colorimetric modifications of the procedure are of
The CoY-2 was generated in the electrode cavity by reduction of 1.0 X 1C-2F CoYwhich is a substitution-inert complex. The solution contained 0.50F NaBr to increase the reversibility of the CoY-2 oxidation (1). The experiment consisted of generating CoY-2 for a measured time, tf, turning off the current for time, td, and then reversing the direction of current flow and recording an anodic chronopotentiogram corresponding to the amount of CoY-2 which had not reacted with the excess Ni+2 ion. The
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