The aim of this paper was to analyze selected properties of beech wood (Fagus sylvatica L.) treated by one-sided surface charring. Specimens were one-side charred with a hot plate using several time-temperature combinations (from 200 to 400 °C). Characteristics such as colour, discoloration, surface roughness, fire resistance, total carbohydrate content at several wood layers and decay resistance were evaluated. Surface charring was applied to the radial and tangential surfaces. Colour measurements showed that the surface of the wood turned grey due to charring. In addition to colour measurements, other experiments showed significant differences between radial and tangential specimens due to their different structures. The higher the temperature used in treating them, the lower the roughness values for radial specimens, while the trend for tangential specimens was the opposite. A smoother surface is more fire resistant, so radial specimens are generally better in this regard. Tangential specimens are more susceptible during preparation to forming cracks that impair flame resistance because a continuous protective densified layer is not formed. The determination of total carbohydrates revealed significant changes at various wood depths after surface charring. These changes were more predictable in radial specimens due to the annual ring orientation, because each layer consisted of a similar earlywood/latewood ratio. Finally, when decay resistance was assessed, weight loss was found to be lower in all specimens than in the references. The results suggest that charring at a particular combination of temperature and time improved the investigated properties of the surface-modified beech.
Strength loss caused by fungal degradation is an important factor to be considered during tree-stability assessment. Detailed information on the relationship between static mechanical properties in relation to the heterogeneity of density and dynamic mechanical parameters of wood degraded by the soft-rot fungus Kretzschmaria deusta can improve the understanding of its decay process and the interpretation of results obtained from stress-wave-based non-destructive methods used for tree-stability assessment. This research presents density profiles of artificially inoculated samples with K. deusta and static mechanical properties of green beech wood in relation to physical parameters (density, moisture content, vibroacoustic parameters). A statistically relevant difference (p < 0.01) in the variability of density distribution between degraded and intact samples was proved. Relevant correlations were proved among modulus of rupture ( M O R $MOR$ ), mass loss and variability longitudinal density distribution. A strong linear relationship between M O R $MOR$ and static modulus of elasticity ( M O E $MOE$ ) of degraded and intact specimens was presented. A strong relationship was also proved between M O R $MOR$ and dynamic parameters (dynamic modulus of elasticity ( M O E D $MOED$ ) and stress-wave velocity in longitudinal direction ( c l ${c}_{l}$ )). M O E D $MOED$ showed a stronger correlation to M O R $MOR$ than c l ${c}_{l}$ proving the importance of density in assessing strength loss through non-destructive methods.
One-sided surface charred European beech wood (Fagus sylvatica L.) was studied. Radial and tangential specimens of dimensions of 50 × 25 × 350 mm were one-sided surface charred at 200, 250, 300, 350, and 400 °C for various times using a contact heating system. Specimens of dimensions of 50 × 25 × 50 mm3 were prepared for treatment intensity analysis and its effect on surface wettability. Density profiles of the radial and tangential charred specimens were determined using X-ray densitography with a resolution of 0.05 mm. The wettability of the one-sided surface charred wood specimens was analyzed via contact angle, measured using the sessile drop method and determined over 10 to 150 s. The oven-dried specimens were partially submerged in water and water uptake was recorded after 2, 4, 6, 8, 10, 48, and 72 h according to EN-927-5. The surface density of the radial specimen groups charred at 200 °C for 6 min and 250 °C for 4 min decreased by about 4.5 to 8.2%. With increasingly severe charring, the surface density decreased by about 15.5 to 33.5%. A mild charring process produced a surface charred layer of approx. 2 mm, while higher temperatures and longer times affected the density up to 4–6 mm beneath the surface. Differences were found between the water uptake of the radial and tangential charred beech specimens. The most significant decrease of 56% in water uptake was recorded for the radial group prepared at 200 °C for 20 min after floating in water for 72 h. Water uptake in the radial groups modified at 250 °C for 4 and 6 min after 72 h decreased by 38% and 36%, respectively. The tangential groups did not show any statistically significant decrease. The average water uptake of the groups charred at 200 °C for 20 min, 350 °C for 2 min and 400 °C for 1 min was greater than that of the reference; the variability of the measured data was significantly greater due to the highly anisotropic character of the tangential specimens. Micro cracks were also visible on the surface. Concluding from the results of this study, one-sided surface charred beech wood exhibits increased potential in terms of wood–water related properties when a temperature range of 200–400 °C is applied.
Wood-decaying fungi are responsible for the degradation of wood and the alteration in its material properties. Fomes fomentarius (L.) Fr. is one of the most common white-rot fungi colonising coarse wood and standing trees. In recent years, according to their genetic, physiological, and morphological differences, Fomes inzengae (Ces. and De Not.) Lécuru was identified as an independent species. This article aimed to compare the impact of the degradation caused by both species on the anatomical, physical, and mechanical properties of beech wood. When comparing the degradation caused by different strains of both species, no statistically significant difference was found in mass loss (ML) or moisture content (MC). A relevant correlation between ML and MC was confirmed for both species. Variabilities in the density distribution of the degraded and intact bending samples were found to be statistically different. No relevant difference was observed in the modulus of rupture (MOR) between the two species after each exposure period. A strong linear relationship between the MOR and the dynamic modulus of elasticity was revealed for both species. Both species showed decay patterns typical for simultaneous white rot and soft rot. According to the presented results, the impact of both species on the investigated material properties of wood cannot be considered significantly different.
Surface carbonization, or charring, of wooden exterior cladding boards is a modification method that creates a fully organic barrier layer in resemblance to a coating. The process effectively degrades the wood and transforms it into a carbonaceous residue that protects the underlying unmodified wood from environmental stresses. The surface quality of wood modified in this manner is a combination of several factors and depends on the manufacturing method and wood species. To assess the quality of spruce and birch modified with contact and flame charring techniques, several experiments were set up from the nanoscale to macroscopic evaluation of surface resistance to different stresses. The degree of changes in elemental composition scale with the modification severity with little differences between wood species. The carbon structures analyzed by high resolution transmission electron microscopy (HR-TEM) were found to be amorphous, but the electron energy loss spectroscopy (EELS) revealed higher ordering with what is assumed to be random graphitic stacking of carbon sheets. These carbon-carbon bonds are stable, so a higher ordering is hypothesized to induce improved resistance to exterior stresses. The scanning electron microscopy (SEM) revealed a clear difference between contact charred and flame charred woods. The selected contact charring temperature was not high enough to induce the transformation of cell walls from anisotropic into an isotropic material but provided other benefits such as a relatively crack-free, smooth and scratch resistant surface. Surface roughness was able to adequately predict the surface quality of the contact charred samples and scratch tests were found to be suitable for evaluating the mechanical stress resistance of the surface instead of abrasion. In terms of overall quality, birch instead of spruce was concluded to better respond to both charring methods, although contact charring eliminates some species-specific characteristics, resulting in more homogeneous surfaces.
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