Mechanical milling was performed on the alloy CrnFeB. X-ray diFSraction and Mlissbauer spectmscopy were used IO follow the progress of the shuctural variation. The experimental results can be interpreted by assuming that the milled powden are composed of a small amount of crystalline component and two disordered components: one with a &om densely packed shucLure and the 0 t h with a random lwsely packed structure. Moreover, differential scanning d o r i m e y was used to obIain the crystallization temperature. A mechanism was proposed la describe the formation of Ihe disordered sttuctwes as well as Ihe structural stability in this alloy.
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