Plasmonic optical fiber sensors are continuously developed for (bio)chemical sensing purposes. Recently, surface plasmon resonance (SPR) generation was achieved in gold-coated tilted fiber Bragg gratings (TFBGs). These sensors probe the surrounding medium with near-infrared narrowband resonances, which enhances both the penetration depth of the evanescent field in the external medium and the wavelength resolution of the interrogation. They constitute a unique configuration to probe all the fiber cladding modes individually. We use them to analyze the modal distribution of gold-coated telecommunication-grade optical fibers immersed in aqueous solutions. Theoretical investigations with a finite-difference complex mode solver are confirmed by experimental data obtained on TFBGs. We show that the refractometric sensitivity varies with the mode order and that the global SPR envelope shift in response to surrounding refractive index (SRI) changes higher than 1e-2 RIU (refractive index unit) can be ~25% bigger than the local SPR mode shift arising from SRI changes limited to 1e-4 RIU. We bring clear evidence that the optimum gold thickness for SPR generation lies in the range between 50 and 70 nm while a cladding diameter decrease from 125 µm to 80 µm enhances the refractometric sensitivity by ~20%. Finally, we demonstrate that the ultimate refractometric sensitivity of cladding modes is ~550 nm/RIU when they are probed by gold-coated TFBGs.

The effective indices of the cladding modes of optical fibers depend on the refractive index of the medium surrounding the fiber. We show experimentally and theoretically that while cladding modes with similar effective indices normally have similar refractometric sensitivities, the addition of a 50 nm thick gold sheath enhances the sensitivity of some EH modes by more than one order of magnitude while nearly completely suppressing the sensitivity of neighbouring HE modes (by three orders of magnitude, down to insignificant levels). A differential sensitivity of ∼1000 nm/(refractive index unit) is experimentally reported between adjacent EH and HE grating resonances.

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The high-order cladding modes of conventional single mode fiber come in semi-degenerate pairs corresponding to mostly radially or mostly azimuthally polarized light. Using tilted fiber Bragg gratings to excite these mode families separately, we show how plasmonic coupling to a thin gold coating on the surface of the fiber modifies the effective indices of the modes differently according to polarization and to mode order. In particular, we show the existence of a single "apolarized" grating resonance, with equal effective index for all input polarization states. This special resonance provides direct evidence of the excitation of a surface plasmon on the metal surface but also an absolute wavelength reference that allows for the precise localization of the most sensitive resonances in refractometric and biochemical sensing applications. Two plasmon interrogation methods are proposed, based on wavelength and amplitude measurements. Finally, we use a biotin-streptavidin biomolecular recognition experiment to demonstrate that differential spectral transmission measurements of a fine comb of cladding mode resonances in the vicinity of the apolarized resonance provide the most accurate method to extract information from plasmon-assisted Tilted fiber Bragg gratings, down to pM concentrations and at least 10(-5) refractive index changes.

We report, for the first time, the use of a surface plasmon resonance (SPR) fiber-optic immunosensor for selective cellular detection through membrane protein targeting. The sensor architecture lies on gold-coated tilted fiber Bragg gratings (Au-coated TFBGs) photoimprinted in the fiber core via a laser technique. TFBGs operate in the near-infrared wavelength range at ∼1550 nm, yielding optical and SPR sensing characteristics that are advantageous for the analyses of cellular bindings and technical compatibility with relatively low-cost telecommunication-grade measurement devices. In this work, we take consider their numerous assets to figure out their ability to selectively detect intact epithelial cells as analytes in cell suspensions in the range of 2-5 × 10(6) cells mL(-1). For this, the probe was first thermally annealed to ensure a strong adhesion of the metallic coating to the fiber surface. Its surface was then functionalized with specific monoclonal antibodies via alkanethiol self-assembled monolayers (SAMs) against extracellular domain of epidermal growth factor receptors (EGFRs) and characterized by peak force tapping atomic force microscopy. A differential diagnosis has been demonstrated between two model systems. The developed immunosensors were able to monitor, in real time, the specific attachment of single intact cells in concentrations from 3 × 10(6) cells mL(-1). Such results confirm that the developed probe fits the lab-on-fiber technology and has the potential to be used as a disposable device for in situ and real-time clinical diagnosis.

The generation of near-IR surface plasmon resonance in gold-coated tilted fiber Bragg gratings is strongly dependent on both the polarization state of the transmission light and the property of confining materials (including the coating materials and surrounding media). These dependencies can be advantageously used to demodulate the amplitude spectrum and retrieve the surrounding refractive index. In this paper, we present an automated demodulation technique that measures the surrounding refractive index by comparing the differential amplitude of resonance peaks near the plasmon attenuation for two orthogonal amplitude spectra recorded in the same operating conditions. A mean sensitivity of more than 500 nm per refractive index unit is reported. This new refractive index measurement method is shown to be accurate to 5×10(-5) over a full range of 0.01 in water solutions.

Highly localized refractive index modulations are photo-written in the core of pure silica fiber using point-by-point focused UV femtosecond pulses. These specific gratings exhibit a comb-like transmitted amplitude spectrum, with polarization-dependent narrowband cladding mode resonances. In this work, eccentric gratings are surrounded by a gold sheath, allowing the excitation of surface plasmon polaritons (SPP) for radially-polarized light modes. The spectral response is studied as a function of the surrounding refractive index and a maximum sensitivity of 50  nm/RIU (refractive index unit) is reported for a well-defined cladding-mode resonance among the spectral comb. This novel kind of plasmonic fiber grating sensor offers rapidity of production, design flexibility, and high temperature stability.