The two-phase flow of a hydrophobic ionic liquid and water was studied in capillaries made of three different materials (two types of Teflon, FEP and Tefzel, and glass) with sizes between 200 μm and 270 μm. The ionic liquid was 1-butyl-3-methylimidazolium bis{(trifluoromethyl)sulfonyl}amide, with density and viscosity of 1420 kg m-3 and 0.041 kg m-1 s-1 , respectively. Flow patterns and pressure drop were measured for two inlet configurations (T-and Y-junction), for total flow rates of 0.065-214.9 cm 3 h-1 and ionic liquid volume fractions from 0.05 to 0.8. The continuous phase in the glass capillary depended on the fluid that initially filled the channel. When water was introduced first, it became the continuous phase with the ionic liquid forming plugs or a mixture of plugs and drops within it. In the Teflon microchannels, the order that fluids were introduced did not affect the results and the ionic liquid was always the continuous phase. The main patterns observed were annular, plug, and drop flow. Pressure drop in the Teflon microchannels at a constant ionic liquid flow rate, was found to increase as the ionic liquid volume fraction decreased, and was always higher than the single phase ionic liquid value at the same flow rate as in the two-phase mixture. However, in the glass microchannel during plug flow, pressure drop for a constant ionic liquid flow rate was always lower than the single phase ionic liquid value. A modified plug flow pressure drop model using a correlation for film thickness derived for the current fluids pair showed very good agreement with the experimental data.
Often, impellers almost as large as the tanks containing them and impeller blades equipped with holes are adopted in industry. In this work, we studied experimentally the main features of the flow generated by this type of impellers for a mixture of glycerol with a carbomeric gel by means of particle image velocimetry. The experiments were conducted at temperatures ranging from 40 to 60°C and impeller speeds ranging from 40 to 140 rpm. In all cases, the flow regime was laminar or in the transition region. We also used computational fluid dynamics simulations to describe the behaviour of the mixer, validating the results experimentally with good agreement. We used the numerical results to obtain information on the performance of the mixer, determining the locations and size of vigorous agitation zones and the local effect of the holes present on the impeller blades. The power curves of the mixer were obtained, and the mixer efficiency in terms of power consumption was found to be similar to other impellers used to mix highly viscous non-Newtonian fluids.
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