We carried out hydrostatic pressure demagnetization experiments up to 1.24 GPa on samples of terrestrial and extraterrestrial rocks and minerals of different lithologies as well as on synthetic samples. The magnetic remanence of samples was measured directly under pressure using a non-magnetic high pressure cell of piston-cylinder type that was inserted into a high sensitivity SQUID magnetometer. In order to bring light on the pressure demagnetization effect, we investigated 50 samples with different magnetic mineralogies, remanent coercivities (B cr) and hysteresis parameters. The samples consisted of pyrrhotite-, magnetite-and titanomagnetite-bearing Martian meteorites, taenite-, tetrataenite and kamacite-bearing ordinary chondrites and pyrrhotite-bearing Rumuruti chondrite; magnetite-and titanomagnetite-bearing basalts, andesites, ignimbrites, obsidians and granites; a variety of pyrrhotite-and hematite-bearing rocks and minerals (jasper, schist, rhyolite, radiolarite); samples of goethite and greigite as well as synthetic samples of dispersed powders of magnetite, hematite, pyrrhotite and native iron set into epoxy resin. Under hydrostatic pressure of 1.24 GPa, applied in a low magnetic field (<5µT), the samples lost up to 84% of their initial saturation isothermal remanent magnetization (SIRM) without any changes in their intrinsic magnetic properties. We found that the efficiency of the pressure demagnetization is not exclusively controlled by the magnetic hardness of the samples (B cr), but that it is strongly dependent on their magnetic mineralogy. For a given magnetic mineralogy the resistance to hydrostatic pressure is roughly proportional to ln(B cr). It was shown that there is no simple equivalence between pressure demagnetization and alternating field demagnetization effects. The
[1] We performed hydrostatic pressure demagnetization experiments up to 1.3 GPa on Martian meteorites: nakhlite NWA998 (magnetite-bearing), basaltic shergottites NWA1068 (pyrrhotite-bearing) and Los Angeles (titanomagnetite-bearing) as well as terrestrial rocks: rhyolite (hematite-bearing) and basalt (titanomagnetite-bearing), using a new non-magnetic highpressure cell. The detailed description of measuring techniques and experimental set-up is presented. We found that under 1.3 GPa the samples lost up to 54% of their initial saturation isothermal remanent magnetization (IRM). Repeated loading resulted in a further decrease of magnetization of the samples. Our experiments show that the resistance of IRM to hydrostatic pressure is not exclusively controlled by the remanent coercivity of the sample, but is strongly dependant on its magnetic mineralogy. There is no simple equivalence between pressure demagnetization and alternating field demagnetization. The extrapolation of these results of pressure demagnetization of IRM of Martian meteorites to the demagnetization of the Martian crust by impacts is discussed. Citation: Bezaeva, N. S., P. Rochette, J. Gattacceca, R. A. Sadykov, and V. I. Trukhin (2007), Pressure demagnetization of the Martian crust: Ground truth from SNC meteorites, Geophys. Res. Lett., 34, L23202,
We describe here a compact nonmagnetic composite high pressure cell of piston-cylinder type with inner diameter of 6 mm equipped with manganin pressure sensor. This cell was developed for room temperature measurements of magnetic remanence of relatively large rock samples (up to 5.8 mm in diameter and 15 mm long cylinders) under hydrostatic pressure up to 1.5 GPa (the operating pressure limit) in the 2G Enterprises superconducting quantum interference device magnetometer. Its design was focused on minimizing the remanent magnetic moment m(r) of the cell (m(r)=3 x 10(-8) A m(2)) that allowed direct measurements of remanent magnetic moment M(r) under pressure for weakly magnetic materials-rock samples (M(r) epsilon[5 x 10(-7),10(-4)] A m(2)). The inner part of this composite cell is made of hard "Russian alloy" (Ni(57)Cr(40)Al(3)) whereas the envelope of the cell corps is made of less magnetic titanium alloy. This design solution permitted to reduce the total remanent magnetic moment of the whole cell and represents the main device feature. We describe here the choice of materials for pressure cell based on their magnetic and mechanical properties, the choice of the pressure transmitting medium (polyethilsiloxane liquid) providing perfectly hydrostatic conditions for the sample as well as the cell geometry. The cell performance is illustrated by results of pressure demagnetization experiments on rocks and minerals.
Abstract-We carried out shock experiments on macroscopic spherical samples of the L4 ordinary chondrite Saratov (natural shock stages S2-S3), using explosively generated spherical shock waves with maximum peak pressures of 400 GPa and shock-induced temperatures >800°C (up to several thousands°C). The evolution of shock metamorphism within a radius of the spherical samples was investigated using optical and scanning electron microscopy, microprobe and magnetic analyses as well as Mo¨ssbauer spectroscopy and X-ray diffraction techniques. Petrographic analyses revealed a shock-induced formation of three different concentric petrographic zones within the shocked samples: zone of total melting (I), zone of partial melting (II), and zone of solid-state shock features (III). We found a progressive pressure-induced oxidation of Fe-Ni metal, whose degree increased with increasing shock peak pressure. The amount of FeO within zone I increased the factor of 1.4 with respect to its amount in the unshocked Saratov sample. This suggests that within zone I about 70 wt% of the initial metallic iron was oxidized, whereas magnetic analyses showed that about 10 wt% of it remained intact. This strongly supports the hypothesis that, in addition to oxidation, a migration of metallic iron from the central heavily shocked zone I toward less shocked peripheral zone took place as well (likely through shock veins where metallic droplets were observed). Magnetic analyses also showed a shock-induced transformation of tetrataenite to taenite within all shocked subsamples, resulting in magnetic softening of these subsamples (decrease in remanent coercivity). These results have important implications for extraterrestrial paleomagnetism suggesting that due to natural impact processes, the buried crustal rocks of heavily cratered solid solar system bodies can have stronger remanent magnetism than the corresponding surface rocks.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.
customersupport@researchsolutions.com
10624 S. Eastern Ave., Ste. A-614
Henderson, NV 89052, USA
Copyright © 2024 scite LLC. All rights reserved.
Made with 💙 for researchers
Part of the Research Solutions Family.