X-ray diffraction analysis of the Rocknest scoop sample is described in (23); similar analyses were performed for John Klein and Cumberland. John Klein and Cumberland were the first two drill samples collected by Curiosity. All scooped or drilled samples pass through the Collection and Handling for In situ Martian Rock Analysis (CHIMRA) sample collection and processing system (10). All powders for X-ray diffraction are processed through a 150-m sieve before delivering a portion to the CheMin inlet funnel.The sieved drill powders were placed into sample cells with 6 μm thick Mylar® windows. Mylar® contributes a minor, broad scattering signature in diffraction patterns that is generally "swamped" by diffraction from the loaded sample. In addition, an aluminized light shield also contributes "peaks" to the observed diffraction patterns. Only ~10 mm 3 of material is required to fill the active volume of the sample cell, which is a disc-shaped volume 8 mm in diameter and 175 m thick. A collimated ∼70 μm diameter X-ray beam illuminates the center of the sample cell. A piezoelectric vibration system on each cell pair shakes the material during analysis, causing grains in the cell to pass through the X-ray beam in random orientations.CheMin measures XRD and XRF data simultaneously using Co radiation in transmission geometry (11). The instrument operates in single-photon counting mode so that between each readout the majority of CCD pixels are struck by either a single X-ray photon or by no photons. In this way, the system can determine both the energy of the photons striking the CCD (XRF) and the two-dimensional (2-D) position of each photon (XRD). The energy and positional information of detected photons in each frame are summed over repeated 10-sec measurements into a "minor frame" of 30 min of data (180 frames). The 2-D distribution of Co K X-ray intensity represents the XRD pattern of the sample. Circumferential integration of these rings, corrected for arc length, produces a conventional 1-D XRD pattern. For conversion of the 2-D CCD pattern to a 1-D pattern we have used FilmScan © software from Materials Data, Inc.CheMin generally operates for only a few hours each night, when the CCD can be cooled to its lowest temperature, collecting as many minor frames as possible for the available analysis time, usually five to seven per night. XRD data were acquired over multiple nights for the John Klein and Cumberland drill samples to provide acceptable counting statistics. Total data collection times were 33.9 hr for John Klein and 20.2 hr for Cumberland. The data for individual minor frames and for each night's analysis were examined separately, and there was no evidence of any changes in instrumental parameters as a function of time over the duration of these analyses. Before sample delivery and analysis, the empty cell was analyzed to confirm that it was indeed empty before receiving the sample. The flight instrument was calibrated on the ground before flight using a quartz-beryl standard, and measurement of this st...

NASA’S Origins, Spectral Interpretation, Resource Identification, and Security–Regolith Explorer (OSIRIS-REx) spacecraft recently arrived at near-Earth asteroid (101955) Bennu, a primitive body that represents the objects that may have brought prebiotic molecules and volatiles such as water to Earth [ 1 ]. Bennu is a low-albedo B-type asteroid [ 2 ] that has been linked to organic-rich hydrated carbonaceous chondrites [ 3 ]. Such meteorites are altered by ejection from their parent body and contaminated by atmospheric entry and terrestrial microbes. Thus, the primary mission objective is to return a sample of Bennu to Earth that is pristine, i.e., not affected by these processes [ 4 ]. The OSIRIS-REx spacecraft carries a sophisticated suite of instruments to characterize Bennu’s global properties; support selection of a sampling site; and document that site at sub-centimeter scales [ 5 - 11 ]. Here we consider early observations to understand how Bennu’s properties compare to pre-encounter expectations and the prospects for sample return. The bulk composition of Bennu appears to be hydrated and volatile-rich, as expected. However, in contrast to pre-encounter modeling of Bennu’s thermal inertia [ 12 ] and radar polarization ratios [ 13 ]—which indicated a generally smooth surface covered by centimeter-scale particles—resolved imaging reveals an unexpected surficial diversity. The albedo, texture, particle size, and roughness are beyond the spacecraft design specifications. On the basis of our pre-encounter knowledge, we developed a sampling strategy to target 50-m-diameter patches of loose regolith with grain sizes less than 2 cm [ 4 ]. We observe only a small number of apparently hazard-free regions, on the order of 5 to 20 meters in extent, the sampling of which poses a substantial challenge to mission success.

International audienceA core flow test autoclave has been designed in order to reproduce an injection well at a scale of 1/20. This autoclave allows the CO2 injection into a steel tube cemented to a core sample of red sandstone from the Triassic formations of Lorraine (France). Temperature and pressure gradients can be recorded between the injection point and the confining water phase. Such gradients imply solubility gradients of CO2 and mineral species into the water phase as permeability changes with time. Some chemical reactions can be observed from collected sample at the end of the experiment. Precipitation and dissolution are suspected both into the cement and rock phases. No fracturing is observed. Cement-rock interface is not opened

The Mars Science Laboratory rover Curiosity scooped samples of soil from the Rocknest aeolian bedform in Gale crater. Analysis of the soil with the Chemistry and Mineralogy (CheMin) x-ray diffraction (XRD) instrument revealed plagioclase (~An57), forsteritic olivine (~Fo62), augite, and pigeonite, with minor K-feldspar, magnetite, quartz, anhydrite, hematite, and ilmenite. The minor phases are present at, or near, detection limits. The soil also contains 27 ± 14 weight percent x-ray amorphous material, likely containing multiple Fe(3+)- and volatile-bearing phases, including possibly a substance resembling hisingerite. The crystalline component is similar to the normative mineralogy of certain basaltic rocks from Gusev crater on Mars and of martian basaltic meteorites. The amorphous component is similar to that found on Earth in places such as soils on the Mauna Kea volcano, Hawaii.

The MIT Faculty has made this article openly available. Please share how this access benefits you. Your story matters. CitationHamilton, V.E., et al., "Evidence for widespread hydrated minerals on asteroid (101955) Bennu." Nature astronomy 3, 4 (2019): p.

Christensen, P. R.; Drouet d'Aubigny, C. Y.; Hamilton, V. E.; Reuter, D. C.; Rizk, B.; Simon, A. A.; Asphaug, E.; Bandfield, J. L.; Barnouin, O. S.; Barucci, M. A.; Bierhaus, E. B.; Binzel, R. P.; Bottke, W. F.; Bowles, N. E.; Campins, H.; Clark, B. C.; Clark, B. E.; Connolly, H. C.; Daly, M. G.; Leon, J. de; Delbo', M.; Deshapriya, J. D. P.; Elder, C. M.; Fornasier, S.; Hergenrother, C. W.; Howell, E. S.; Jawin, E. R.; Kaplan, H. H.; Kareta, T. R.; Le Corre, L.; Li, J.-Y.; Licandro, J.; Lim, L. F.; Michel, P.; Molaro, J.; Nolan, M. C.; Pajola, M.; Popescu, M.; Garcia, J. L. Rizos; Ryan, A.; Schwartz, S. R.; Shultz, N.; Siegler, M. A.; Smith, P. H.; Tatsumi, E.; Thomas, C. A.; Walsh, K. J.; Wolner, C. W. V.; Zou, X.-D. and Lauretta, D. S. (2019). Properties of rubble-pile asteroid (101955) Bennu from OSIRIS-REx imaging and thermal analysis. Nature Astronomy, 3 pp. 341-351. For guidance on citations see FAQs.Length of main text: 2956 words Length of methods: 3605 words Length of legends: 565 words Number of references: 53 main text, 69 including methods and supplementary information (refs 67 to 69 are cited in the SI only) , we show that asteroid (101955) Bennu's surface is globally rough, dense with boulders and low in albedo. The number of boulders is surprising given Bennu's moderate thermal inertia, suggesting that simple models linking thermal inertia to particle size do not adequately capture the complexity relating these properties. At the same time, we find evidence for a wide range of particle sizes with distinct albedo characteristics. Our findings imply that ages of Bennu's surface particles span from the disruption of the asteroid's parent body (boulders) to recent in situ production (micron-scale particles).

The Open University's repository of research publications and other research outputs The dynamic geophysical environment of (101955) Bennu based on OSIRIS-REx measurements

Abstract-We review the results of an extensive campaign to determine the physical, geological, and dynamical properties of asteroid (101955) Bennu. This investigation provides information on the orbit, shape, mass, rotation state, radar response, photometric, spectroscopic, thermal, regolith, and environmental properties of Bennu. We combine these data with cosmochemical and dynamical models to develop a hypothetical timeline for Bennu's formation and evolution. We infer that Bennu is an ancient object that has witnessed over 4.5 Gyr of solar system history. Its chemistry and mineralogy were established within the first 10 Myr of the solar system. It likely originated as a discrete asteroid in the inner Main Belt approximately 0.7-2 Gyr ago as a fragment from the catastrophic disruption of a large (approximately 100-km), carbonaceous asteroid. It was delivered to near-Earth space via a combination of Yarkovsky-induced drift and interaction with giant-planet resonances. During its journey, YORP processes and planetary close encounters modified Bennu's spin state, potentially reshaping and resurfacing the asteroid. We also review work on Bennu's future dynamical evolution and constrain its ultimate fate. It is one of the most Potentially Hazardous Asteroids with an approximately 1-in-2700 chance of impacting the Earth in the late 22nd century. It will most likely end its dynamical life by falling into the Sun. The highest probability for a planetary impact is with Venus, followed by the Earth. There is a chance that Bennu will be ejected from the inner solar system after a close encounter with Jupiter. OSIRIS-REx will return samples from the surface of this intriguing asteroid in September 2023.