Iminophosphoranes are reported as convenient precursors to amides,
ureas, carbamates and other carbonyl-containing molecules through
CO2-fixation. Key to this transformation with stable isotopes and
carbon-11 is interception of the reactive isocyanate intermediate.
Automated synthesis and isolation of PET radiopharmaceuticals is
achieved.
Iminophosphoranes are reported as convenient precursors to amides,
ureas, carbamates and other carbonyl-containing molecules through
CO2-fixation. Key to this transformation with stable isotopes and
carbon-11 is interception of the reactive isocyanate intermediate.
Automated synthesis and isolation of PET radiopharmaceuticals is
achieved.
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