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The reaction of 5H,7H-dibenzo[b,g][1,5]ditellurocin with I2 resulted in the formation of the diiodo-ditellurane as a new class of bis-hypervalent chalcogenide. Treatment of the dibromo-derivative of 5H,7H-dibenzo[b,g][1,5]telluraselenocin with aqueous NaOH solution afforded exclusively the telluroxide which showed the strong transannular hypervalent interaction between the tellurinyl group and the selenyl group as evidenced by 77Se and 125Te NMR spectroscopy.
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