Dip-in direct-laser-writing (DLW) optical lithography allows fabricating complex three-dimensional microstructures without the height restrictions of regular DLW. Bow-tie elements assembled into mechanical metamaterials with positive/zero/negative Poisson's ratio and with sufficient overall size for direct mechanical characterization aim at demonstrating the new possibilities with respect to rationally designed effective materials.
In this work, the mechanical behaviour of millimetre-scale, bulk single crystalline, nanoporous gold at room temperature is reported for the first time. Tension and compression tests were performed with a custom-designed test system that accommodates small-scale samples. The absence of grain boundaries in the specimens allowed measurement of the inherent strength of millimetre-scale nanoporous gold in tension. The elastic modulus and strength values in tension and compression were found to be significantly lower than values measured with nanoindentation-based techniques and previously reported in the literature, but close to those reported for millimetre-scale polycrystalline samples tested using traditional compression techniques. Fracture toughness was found to be very low, in agreement with the macroscopic brittleness of nanoporous gold, but this is due to the localization of deformation to a narrow zone of ligaments, which individually exhibit significant plasticity and necking
Micro electro mechanical systems, coatings, and thin films contain materials that are often subjected to complex loading conditions and high frequencies. Therefore, the implementation of a resonant multiaxial fatigue setup for small-scale samples is of high interest. Finite Element simulations have been used to design small-scale samples which possess very close bending and torsional resonant frequencies.The bending and torsional modes are excited by two piezo actuators working either in or out of phase with one another. The bending and torsional amplitudes are measured independently by a laser and the actuator amplitudes are controlled by a Field Programmable Gate Array. The fatigue setup can be used with a varying range of sample sizes from centimeters down to tens of micrometers. The novel multiaxial resonant micro fatigue setup as well as results (fatigue damage for Ni and lifetime for Cu) from bending small-scale fatigue tests are shown and discussed.
Inhalt: Für die Auslegung von Bauteilen ist die Bewertung der Schädigungsinitiierung von ausschlaggebender Bedeutung. Insbesondere bei zyklischen Betriebsbeanspruchungen ist zu prognostizieren, ob die vorliegende Mikrostruktur weiteres Risswachstum eher begünstigt oder mindert. In Schweißverbindungen ist eine Bewertung aufgrund der prozessbedingt unterschiedlichen Gefügestrukturen besonders schwierig. An Mikroproben hat das Fraunhofer-Institut für Werkstoffmechanik IWM die Rissentstehungsphase in Schweißverbindungen untersucht und ein probabilistisches Bewertungskonzept entwickelt. Das neue Verfahren vermeidet unnötige Konservativitäten und liefert damit eine Verbesserung der Materialausnutzung.
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