A testing programme was conducted to investigate the material properties of a new highchromium grade of austenitic stainless steel-EN 1.4420 at elevated temperatures. A total of 164 tensile coupons extracted from both cold-rolled and hot-rolled sheets were tested; 80 coupons were tested isothermally with temperatures ranging from 25 °C to 1100 °C, and 84 were tested anisothermally with stress levels ranging from 10% to 90% of the material 0.2% proof stress at room temperature. The experimentally derived reduction factors for the key material properties were compared with existing design values. Design recommendations for the elevated temperature reduction factors were then proposed for this new grade, and a twostage Ramberg-Osgood model was shown to be able to accurately represent the material stressstrain response at elevated temperature.

This report addresses the origin of peculiar anisotropic deformation of sapphire. The three-dimensional finite element simulation of the contact between spherical indenter and elastically anisotropic solid allowed us to analyze stress under the tip that penetrates in the (1010) and ͑0001͒ planes, and consequently, to localize those regions in which particular deformation mechanisms are likely to be activated. This approach contrasts the available models of ''hardness anisotropy,'' which routinely apply a modified uniaxial-stress approach to this essentially three-dimensional, nonisotropic contact problem. The calculated results are in agreement with the microscopic inspection of impressions; that is, the surface features reflect the distribution of stress. The computations made it also possible to evaluate the actual radius of the tip ͑nominally 5 m ball͒.

Stainless steel material is a suitable choice for modern steel constructions as it has a high resistance to corrosion combined with high material strength and ductility. Furthermore, its use leads to significant reductions in maintenance. In this frame, bolted connections made of stainless steel components become more and more important to enhance the application of stainless steel not only to small parts of steel structures but also to complex structures. Whereas non preloaded stainless steel bolted connections are already widely used, according to EN 1090-2, the application of preloaded stainless steel bolting assemblies is not allowed unless otherwise specified. If they shall be used, they shall be treated as special fasteners and a procedure test is mandatory. Also EN 1993-1-4 requires that their acceptability in a particular application has to be demonstrated from test results. These restrictions are mainly caused by two facts: firstly, the viscoplastic deformation behaviour of stainless steel which might result in not negligible preload losses in the bolting assemblies themselves and secondly, the gap of knowledge regarding suitable tightening parameters and procedures for stainless steel bolting assemblies to secure a required preload in the bolting assemblies and to avoid galling. To solve these questions, research activities have been carried out in the frame of the European RFCS-research project "Execution and reliability of slip resistant connections for steel structures using CS and SS" SIROCO. The present contribution gives an initial insight into the viscoplastic deformation behaviour of stainless steel bolting assemblies which were achieved in SIROCO which shows that preloaded bolted stainless steel connections can be treated similar to those made of carbon steel.

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Scale formation of AISI 304 stainless steel during annealing at temperatures between 1100 and 1200 °C under a water vapor‐containing atmosphere is studied. Characterization of the oxide scale is performed with field‐emission scanning electron microscopy–energy dispersive spectroscopy (FESEM–EDS) and glow discharge optical emission spectroscopy (GDOES) and removal of oxide scale is done via neutral electrolyte pickling. The pickling conditions are kept constant and the effect of the annealing conditions and scale properties on the pickling result are examined. The effectiveness of pickling is evaluated using analysis FESEM images taken on polished sections of pickled surfaces. Research shows that the thickness, morphology, and composition of the oxide scale are dependent on annealing temperature and time. The thicknesses of the scale formed under the established conditions vary from 0.2 to over 30 μm, and morphologies between the chromium rich oxide layer and layered scale structure formed by breakaway oxidation. The pickling response of oxide scales remains good at all annealing temperatures with the shortest exposure time.

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