The performance of particle‐based products depends on a multiple set of particle properties. To monitor them during particle manufacturing, three novel aerosol measurement techniques were developed: wide‐angle light scattering (WALS), three‐dimensional laser scattering (3D‐LSS), and differential aerodynamic particle sizing (DAPS). They measure particle shape, aggregate structure, and particle size, i.e., radius of gyration and aerodynamic diameter. The techniques were tested for rod‐like organic pigments and partially sintered SiO2 aggregates, which were produced by two new aerosol generators.
A novel generator for a defined test aerosol consisting of nonspherical particles was developed based on the desublimation of copper phthalocyanine during adiabatic cooling. Employing a brush disperser, copper phthalocyanine powder is dosed and dispersed in a nitrogen flow and sublimated in a tube furnace. Downstream the furnace new particles are formed due to the adiabatic expansion and the desublimation of the material in a laval nozzle. The generated particles were characterized employing a scanning mobility particle sizer and an aerosol particle mass analyzer to determine the size distribution and the dynamic shape factor. For the operating parameters of the generator examined here, particles with a mobility diameter between 30 and 600 nm were generated. The measured values for the dynamic shape factor of the particles were confirmed by scanning electron microscopy analysis.
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