The study deals with an online monitoring approach for adhesively bonded composite joints. A modification of epoxy-based adhesive films with carbon nanotubes allows for electrical resistance measurements through the bonding via inkjet-printed silver conductive circuits on the composites structure. Impact damages are introduced into adhesively bonded glass fiber–reinforced polymer specimens. In-plane and through-thickness electrical resistance measurements show the possibility of accurate damage detection and damage localization of the introduced damages in one or two dimensions, depending on the conductive path designs. The measured electrical resistance changes are compared with results from ultrasonic inspections and light microscopy observations. Furthermore, a linear correlation of electrical resistance and bond line thickness was found. The results demonstrate the applicability of the presented method in a structural health monitoring system.
The influence of nanoparticle morphology and filler content on the mechanical and electrical properties of carbon nanoparticle modified epoxy is investigated regarding small volumes. Three types of particles, representing spherical, tubular and layered morphologies are used. A clear size effect of increasing true failure strength with decreasing volume is found for neat and carbon black modified epoxy. Carbon nanotube (CNT) modified epoxy exhibits high potential for strength increase, but dispersion and purity are critical. In few layer graphene modified epoxy, particles are larger than statistically distributed defects and initiate cracks, counteracting any size effect. Different toughness increasing mechanisms on the nano- and micro-scale depending on particle morphology are discussed based on scanning electron microscopy images. Electrical percolation thresholds in the small volume fibres are significantly higher compared to bulk volume, with CNT being found to be the most suitable morphology to form electrical conductive paths. Good correlation between electrical resistance change and stress strain behaviour under tensile loads is observed. The results show the possibility to detect internal damage in small volumes by measuring electrical resistance and therefore indicate to the high potential for using CNT modified polymers in fibre reinforced plastics as a multifunctional, self-monitoring material with improved mechanical properties.
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