The unsaponifiable lipid fraction of plant-based foods is a potential source of bioactive components such as phytosterols, squalene, and tocopherols. The objective of the present study was to determine the levels of phytosterols, and squalene, as well as tocopherols (alpha and beta + gamma) in selected grains, seeds, and legumes. The method comprised acid hydrolysis and lipid extraction followed by alkaline saponification, prior to analysis by HPLC. In addition, the fatty acid profile of the foods was determined via total lipid extraction, fatty acid derivitisation and GC analysis. In general, beta-sitosterol was the most prevalent phytosterol, ranging in concentration from 24.9 mg/100 g in pumpkin seed to 191.4 mg/100 g in peas. Squalene identified in all foods examined in this study, was particularly abundant in pumpkin seed (89.0 mg/100 g). The sum of alpha- and beta+ gamma-tocopherols ranged from 0.1 mg/100 g in rye to 15.9 mg/100 g in pumpkin seeds. Total oil content ranged from 0.9% (w/w) in butter beans to 42.3% (w/w) in pumpkin seed and the type of fat, in all foods examined, was predominantly unsaturated. In conclusion, seeds, grains, and legumes are a rich natural source of phytosterols. Additionally, they contain noticeable amounts of squalene and tocopherols, and in general, their fatty acid profile is favorable.

The root-mean-square (rms) nuclear charge radius of 8 He, the most neutron-rich of all particlestable nuclei, has been determined for the first time to be 1.93(3) fm. In addition, the rms charge radius of 6 He was measured to be 2.068(11) fm, in excellent agreement with a previous result.The significant reduction in charge radius from 6 He to 8 He is an indication of the change in the correlations of the excess neutrons and is consistent with the 8 He neutron halo structure. The experiment was based on laser spectroscopy of individual helium atoms cooled and confined in a magneto-optical trap. Charge radii were extracted from the measured isotope shifts with the help of precision atomic theory calculations. * Electronic address: pmueller@anl.gov 1

The commercially available in-clinic ELISA could be used by veterinarians to screen dogs for heartworm infection and for exposure to tick-borne pathogens.

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Measurements of 81Kr/Kr in deep groundwater from the Nubian Aquifer (Egypt) were performed by a new laser‐based atom‐counting method. 81Kr ages range from ∼2 × 105 to ∼1 × 106 yr, correlate with 36Cl/Cl ratios, and are consistent with lateral flow of groundwater from a recharge area near the Uweinat Uplift in SW Egypt. Low δ2H values of the 81Kr‐dated groundwater reveal a recurrent Atlantic moisture source during Pleistocene pluvial periods. These results indicate that the 81Kr method for dating old groundwater is robust and such measurements can now be applied to a wide range of hydrologic problems.

Background: Octupole-deformed nuclei, such as that of 225 Ra, are expected to amplify observable atomic electric dipole moments (EDMs) that arise from time-reversal and parity-violating interactions in the nuclear medium. In 2015, we reported the first "proof-of-principle" measurement of the 225 Ra atomic EDM.Purpose: This work reports on the first of several experimental upgrades to improve the statistical sensitivity of our 225 Ra EDM measurements by orders of magnitude and evaluates systematic effects that contribute to current and future levels of experimental sensitivity. Method: Laser-cooled and trapped225 Ra atoms are held between two high voltage electrodes in an ultra high vacuum chamber at the center of a magnetically shielded environment. We observe Larmor precession in a uniform magnetic field using nuclear-spin-dependent laser light scattering and look for a phase shift proportional to the applied electric field, which indicates the existence of an EDM. The main improvement to our measurement technique is an order of magnitude increase in spin precession time, which is enabled by an improved vacuum system and a reduction in trap-induced heating. Results: We have measured the225 Ra atomic EDM to be less than 1.4 × 10 −23 e cm (95% confidence upper limit), which is a factor of 36 improvement over our previous result. Conclusions:Our evaluation of systematic effects shows that this measurement is completely limited by statistical uncertainty. Combining this measurement technique with planned experimental upgrades we project a statistical sensitivity at the 1 × 10 −28 e cm level and a total systematic uncertainty at the 4 × 10 −29 e cm level.

Laser manipulation of neutral atoms has been used to count individual krypton-85 and krypton-81 atoms present in a natural krypton gas sample with isotopic abundances in the range of 10 −11 and 10 −13 , respectively. This method of isotope trace analysis is free of contamination from other isotopes and elements and can be applied to several different isotope tracers for a wide range of applications. The demonstrated detection efficiency is 1 × 10 −7 . System improvements could increase the efficiency by many orders of magnitude.

We have performed precision laser spectroscopy on individual 6He (t(1/2)=0.8 s) atoms confined and cooled in a magneto-optical trap, and measured the isotope shift between 6He and 4He to be 43 194.772+/-0.056 MHz for the 2(3)S1-3(3)P2 transition. Based on this measurement and atomic theory, the nuclear charge radius of 6He is determined for the first time in a method independent of nuclear models to be 2.054+/-0.014 fm. The result is compared with the values predicted by a number of nuclear structure calculations and tests their ability to characterize this loosely bound halo nucleus.