The increase in awareness towards global warming has prompted the research of alternatives to the conventional ordinary Portland Cement (OPC). The Class G OPC produces huge amounts of carbon dioxide (CO2) gas during its production. The slag based geopolymer cement has been identified as a potential greener alternative. Slag is chosen as the raw material because it contains silica and aluminum which is classified as pozzolan material that can be used to synthesis geopolymer cement. As most of the research done for slag based geopolymer cement is for the construction industry, and therefore, the parameters, ratios and compositions of the cement need to be improved to suit oilwell cementing criteria. The cement was tested for rheology test, fluid loss test and compressive strength test according to API cement testing procedures. The results shown that, 20% volume of water, in 166 Dinesh Kanesan et al.relative to volume of slag and alkali activator produced the optimum density and viscosity result compared to 10% and 30% of water. Meanwhile, Sodium Hydroxide (NaOH) to Sodium Silicate (Na2SiO3) ratio of 1:2.5 gave the ideal result compared to the ratio of 1:0.5, 1:1 and 1:2. Optimum density and viscosity were achieved using NaOH molarity of 12M instead of 10M and 14M. When the slurry with different volume of dispersant were kept for 10 minutes, the thickening time varied. The optimum dispersant volume was 10mL which enabled the slurry to remain in liquid state at the end of the 10 minute test duration.
Objectives, Scope This paper provides valuable insights on aqueous retarded acid system evaluation based on laboratory testing, literature review and engineering analysis prior to the field application for a candidate well in a gas field, offshore East Malaysia (Figure 1). The field is a reefal carbonates build-up overlayed by a thick shale sequence and is one of the deepest fields in Sarawak Asset, in which the produced fluid contains up to 3,500ppm H2S, 20% CO2 and bottomhole temperature up to 288°F. Production enhancement for this carbonate reservoir requires application of a more effective approach to address challenges associated with acid placement and reservoir contact in long pay zones of complex diagenetic facies high temperature carbonate reservoirs, thereby improving return on investment. Figure 1Structural map of Central Luconia carbonate platform offshore Sarawak, Malaysia (Janjuhah et al. 2016) Methods, Procedures, Process The workflow adopted for the stimulation job involves thorough historical production data analysis, detail petrophysical review to evaluate reservoir properties, in-depth production performance analysis (i.e. nodal and network modeling), completion review to ascertain damage mechanism and economic evaluation that include decision risk analysis to evaluate all range of probabilistic outcome. Initial selection of stimulation fluids was based on the mineralogical composition of the main producing formation. A detailed study of reservoir rock and its reaction to various acid systems has been based upon software modeling where sensitivity analyses involving multiple treatment schedule scenarios incorporating various acid and diverter fluid systems are considered. Coreflood experiment was then performed to determine the Pore Volume to Breakthrough (PVBT) comparing emulsified acid with aqueous retarded acid at temperature of 250°F, injection rate of 3ml/min and at confining pressure of 1,500psi. The low PVBT values (i.e. 1.125 and 0.521) and unique breakthrough features obtained from the coreflood confirmed that aqueous retarded acid is effective to stimulate the carbonate reservoir. Compatibility testing was also conducted to assess the stability of the retarded acid recipes and potential reaction with reservoir fluids (i.e. water and condensate), downhole completion and surface equipment. Results, Observation, Conclusion An established stimulation software was used to refine the acid volume calculation and placement analysis. Field trial was made using combined application of the aqueous retarded acid and viscoelastic diverting acid. Considering several case scenarios, the remedial treatment was performed via bullheading to achieve optimum injection rate within 5bpm to 7bpm. Total of 197bbls acid and 197bbls diverter was be pumped during the treatment that will be split in several stages to achieve average invasion profile of 2.8ft and -1.3 skin value. This paper presents aqueous retarded acid system as alternative to widely used emulsified acid systems. Field application of the approach supports the theoretical findings based on substantial improvement in well production, pressure matching of the remedial treatment and calibrated nodal analysis assessment. This demonstrates the value of holistic approach of laboratory testing, comprehensive software modeling and application of enhanced stimulation fluids to overcome complex technical challenges Novel, Additive Information The field production was previously constrained by its high CO2 levels and the supply gas ratio agreement. The information and lessons learnt from this paper will be applicable as evident of practical improvements to achieve sustainable production from the field since it has a strategic importance as production, processing and export hub to other four gas fields. Recent CO2 blending project has allow a better distribution of gas across the network and therefore demand higher production from the field, thus further unlock it potential to achieve economic optimization.
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