From the hydroboration of the unsaturated cluster (p-H)20~3(C0)10 in the presence of tetrahydrofuran, a cluster system was prepared with boroxine (B303) supporting three triosmium units, which was shown to be a useful starting material in the synthesis of the triosmium methylidyne clusters, (p-H)3(CO)gOs3(CCI), (p-H)3(CO)gOs3(CBr), and (p-H)3(CO)90s3(CPh).
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