Nano-or submicron In(OH) 3 and In 2 O 3 particles of different morphologies were synthesized from a nitrate solution by a homogeneous precipitation process. By using X-ray diffractometer, thermogravimetric analysis, transmission and scanning electron microscopes, and inductively coupled plasma-optical emission spectrometry, the properties of particle growth were analyzed. The results indicated that the kinetics of the hydrolysis reaction of In 31 was a zero-order reaction with an activation energy of 128 kJ/mol, which implied that the reaction was controlled by the decomposition kinetic of urea additive. The growth anisotropic of particles, pH value of reaction solutions, residual In 31 concentration relative to aging time with different temperatures and starting concentrations were reported in this study. Calcination of the hydrate to form In 2 O 3 particles between 3001 and 9001C did not greatly change the morphologies of the particles.
527J ournal
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.