This article demonstrates the characterization of field emission from individual carbon nanotubes (CNTs) attached to a tungsten tip, when the separation distance s between the anode and tip of the CNT (cathode) is less than 15μm. The separation distance is adjusted with a nanopositioning stage after establishing a datum by detecting the anode surface with the CNT tip. Our separation distance s differs by the height h of the CNT from the distance d that is often measured between the planar anode and the planar substrate of an emitting cathode. Consequently, the electric field at the tip of the CNT is modeled by F=λV∕s, where λ is our field amplification factor, rather than by F=γV∕d, where γ is the more conventional field enhancement factor. Twenty-four sets of current-voltage I(V) data were measured from an individual multiwall CNT at separation distances s between 1.4 and 13.5μm. A nonlinear curve-fitting algorithm extracted Fowler-Nordheim (FN) parameters from each set of I(V) data, rather than conventional extraction from the FN plots. The turn-on voltage Vto (to emit 1nA) as a function of the separation distance followed an empirical power relation Vto=asb, and the field amplification factor λ empirically followed the relation λ=λ∞s∕(s+h)+1. This experimental characterization is an improvement over other techniques since the gap is controlled more precisely over a larger range, the electric field at the CNT tip is not disturbed by other CNTs, and the anode is flat to within a few nanometers.
Micro scale features are fabricated on Si (100) surfaces using lithographic techniques and then thermally processed in an ultra high vacuum (UHV) environment. Samples are flash heated at 1200 °C and further annealed at 1050 °C for 18 hours. The surface morphology was examined using an atomic force microscopy (AFM). The process resulted in the formation of symmetric, reproducible step-terrace patterns with very wide atomically flat regions exhibiting highly reproducible step-terrace morphology. 25 µm lithographically patterned cells spontaneously transform into a symmetric formation marked by step bunches pinned by pyramidal structures separated by wide atomic terraces. The pyramidal features are visible using a conventional optical microscope and are to be used as fiducial marks to locate nanoscale features fabricated on the atomically flat terraces.
Some metallic alloys such as Nitinol ͑NiTi͒ exhibit the shape memory effect, which is suitable for generating force and displacement when the alloy changes phase during a heating and cooling cycle. These shape memory alloys are often formed into one-dimensional wires, tubes, and ribbons that are preloaded by bias springs to create inexpensive actuators for electromechanical devices. This article describes a new instrument for measuring the quasistatic characteristics of the alloy and the transient performance of bias-spring actuators when resistively heated and convectively cooled. The instrument achieves more accurate measurements by eliminating rolling friction and by sensing force and displacement in line with the bias spring and shape memory alloy wire. Data from the instrument enables calculation of stress and strain at constant temperatures and during actuation cycles.
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