Cu(NO3)(C2H302)(CIoH9N3)], Mr = 355"79, monoclinic, P2~/n, Z=4, a = 12.859(3), b = 9-674 (2), c = 12.247 (3) A., /3 = 113.52 (2) °, V = 1396.93 A. 3, D m (flotation) = 1.720 (6), Dx = 1.692 g cm -3, A(Mo Ka) = 0"71069/~, /z = 15"36 cm -1, T= 298 K, F(000) = 724, 1822 unique observed reflections. R = 0.037.The local molecular CUN2020'2 chromophore involves an elongated rhombic octahedral structure, with nearly symmetrically bonded di-2-pyridylamine (dpyam) and bidentate acetate groups bonding in the plane and bridging 'semi-coordinate' nitrate groups completing the six coordination.
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