Skin pass rolling is considered as the final forming stage in cold‐rolled close annealed steel. Surface properties and flatness are the key attributes for automotive customers. Efficient skin pass rolling overcomes surface defects that lead to material rejection. This study portrays a brown stain defect with higher defect severity. The brown stain defect is observed in a few coils that are processed through alkaline electrocleaning (ECL). Coils bypassing ECL do not show such defect. Defect characterization through scanning electron microscopy, Fourier transform infrared spectroscopy, and Raman spectroscopy shows initiation of oxidation of steel substrate. The presence of skin pass fluid residues in the defected area is the root cause for the stain formation. Techniques such as glow discharge optical emission spectroscopy, Kelvin probe, Raman spectroscopy, and electrochemical tests emphasize the role of final electrode polarity in ECL with the nature of passive oxide film formed when skin pass fluid is applied on the steel surface. This study reveals that skin pass fluid applied on anodically cleaned coils provides a uniform passive surface that restricts the defect formation.
Surface of cold-rolled steel intended for automotive body panel applications is expected to be defect free. The presence of surface defects hampers the aesthetics and average surface roughness and thereby deteriorates the paintability of the steel sheet. This study aims to investigate the source of white patch defect in cold-rolled and skin-passed interstitial free steel sheets. Macroscopic observations of as-received white patch sample revealed the presence of blackish deposit having cracks inside the deposits, suggesting that these deposits were heated up possibly during annealing process. Further during macroscopic observation, it was revealed that the black deposits were of near round shape. If deposit is present before rolling, then it is expected that it will elongate during rolling and will not retain round shape. Round shape of the deposits under investigation suggested that it is not before rolling. Electrolytic cleaning line (ECL) is the only inbetween process. Surface characterization techniques such as SEM-EDS, Raman spectroscopy, Fourier transform infrared spectroscopy were used to analyze the defect and good region of the steel sheet. Overall analysis indicated grease contamination on cold-rolled steel sheet at the entry of ECL caused generation of white patch defect. Regular cleaning and preventive maintenance of plant machinery were recommended to avoid such leakages to arrest the defect generation in the future.
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