International audienceThe objective of this work was to observe and quantify the onset and evolution of localised deformation processes in sand with grain-scale resolution. The key element of the proposed approach is combining state-of-the-art X-ray micro tomography imaging with three-dimensional volumetric digital image correlation techniques. This allows not only the grain-scale details of a deforming sand specimen to be viewed, but also, and more importantly, the evolving three-dimensional displacement and strain fields throughout loading to be assessed. X-ray imaging and digital image correlation have been in the past applied individually to study sand deformation, but the combination of these two methods to study the kinematics of shear band formation at the grain scale is the first novel aspect of this work. Moreover, the authors have developed a completely original grain-scale volumetric digital image correlation method that permits the characterisation of the full kinematics (i.e. three-dimensional displacements and rotations) of all the individual sand grains in a specimen. The results obtained using the discrete volumetric digital image correlation confirm the importance of grain rotations associated with strain localisation

Recent developments in the application of x-ray micro-tomography in laboratory geomechanics have allowed all the individual grains of sand in a test sample to be seen and identified uniquely in 3D. Combining such imaging capabilities with experiments carried out "in-situ" within an imaging setup has lead to the possibility of directly observing the mechanisms of deformation as they happen. The challenge has thus become extracting pertinent, quantified information from these rich time-lapse 3D images to elucidate the mechanics at play. This paper presents a new approach (ID-Track) for the quantification of individual grain kinematics (displacements and rotations) of large quantities of sand grains (tens of thousands) in a test sample undergoing loading. With ID-Track, grains are tracked between images based on some geometrical feature(s) that allow their unique identification and matching between images. This differs from Digital Image Correlation (DIC), which makes measurements by recognising patterns between images. Since ID-Track does not use the image of a grain for tracking, it is significantly faster than DIC. The technique is detailed in the paper, and is shown to be fast and simple, giving good measurements of displacements, but suffering in the measurement of rotations when compared to Discrete DIC. Subsequently, results are presented from successful applications of ID-track to triaxial tests on two quite different sands: the angular Hostun sand and the rounded Caicos Ooids. This reveals details on the performance of the technique for different grain shapes and insight into the differences in the grain-scale mechanisms occurring in these two sands as they exhibit strain localisation under triaxial loading.

Ultrasonic waves propagating in solids have stress-dependent velocities. The relation between stress (or strain) and velocity forms the basis of non-linear acoustics. In homogeneous solids, conventional time-of-flight techniques have measured this dependence with spectacular precision. In heterogeneous media such as concrete, the direct (ballistic) wave around 500 kHz is strongly attenuated and conventional techniques are less efficient. In this manuscript, the effect of weak stress changes on the late arrivals constituting the acoustic diffuse coda is tracked. A resolution of 2 x 10(-5) in relative velocity change is attained which corresponds to a sensitivity to stress change of better than 50 kPa. Therefore, the technique described here provides an original way to measure the non-linear parameter with stress variations on the order of tens of kPa.

No abstract

Interparticle forces in granular materials are intimately linked to mechanical properties and are known to self-organize into heterogeneous structures, or force chains, under external load. Despite progress in understanding the statistics and spatial distribution of interparticle forces in recent decades, a systematic method for measuring forces in opaque, three-dimensional (3D), frictional, stiff granular media has yet to emerge. In this Letter, we present results from an experiment that combines 3D x-ray diffraction, x-ray tomography, and a numerical force inference technique to quantify interparticle forces and their heterogeneity in an assembly of quartz grains undergoing a one-dimensional compression cycle. Forces exhibit an exponential decay above the mean and partition into strong and weak networks. We find a surprising inverse relationship between macroscopic load and the heterogeneity of interparticle forces, despite the clear emergence of two force chains that span the system.

The delineation and characterization of fracturing is important in the successful exploitation of many hydrocarbon reservoirs. Such fracturing often occurs in preferentially aligned sets; if the fractures are of subseismic scale, this may result in seismic anisotropy. Thus, measurements of anisotropy from seismic data may be used to delineate fracture patterns and investigate their properties. Here fracture-induced anisotropy is investigated in the Valhall field, which lies in the Norwegian sector of the North Sea. This field is a chalk reservoir with good porosity but variable permeability, where fractures may significantly impact production, e.g., during waterflooding. To investigate the nature of fracturing in this reservoir, P-wave amplitude variation with offset and azimuth (AVOA) is analyzed in a 3D ocean-bottom cable (OBC) data set. In general, 3D ocean-bottom seismic (OBS) acquisition leads to patchy coverage in offset and azimuth, and this must be addressed when considering such data. To overcome this challenge and others associated with 3D OBS acquisition, a new method for processing and analysis is presented. For example, a surface fitting approach, which involves analyzing azimuthal variations in AVO gradients, is used to estimate the orientation and magnitude of the fracture-induced anisotropy. This approach is also more widely applicable to offset-azimuth analysis of other attributes (e.g., traveltimes) and any data set where there has been true 3D data acquisition, land or marine. Using this new methodology, we derive high-resolution maps of P-wave anisotropy from the AVOA analysis for the top-chalk reflection at Valhall. These anisotropy maps show coherent but laterally varying trends. Synthetic AVOA modeling, using effective medium models, indicates that if this anisotropy is from aligned fracturing, the fractures are likely liquid filled with small aspect ratios and the fracture density must be high. Furthermore, we show that the fracture-normal direction is parallel to the direction of most positive AVO gradient. In other situations the reverse can be true, i.e., the fracture-normal direction can be parallel to the direction of the most negative AVO gradient. Effective medium modeling or comparisons with anisotropy estimates from other approaches (e.g., azimuthal variations in velocity) must therefore be used to resolve this ambiguity. The inferred fracture orientations and anisotropy magnitudes show a degree of correlation with the positions and alignments of larger scale faults, which are estimated from 3D coherency analysis. Overall, this work demonstrates that significant insight may be gained into the alignment and character of fracturing and the stress field variations throughout a field using this highresolution AVOA method.

No abstract

Combining x-ray tomography and three-dimensional (3D) image analysis has finally opened the way for experimental micro-(geo)mechanics, allowing access to different scales of interest. When these correspond to a scale that has been imaged at high spatial resolution, high-quality measurements can be obtained (e.g. 3D displacements and rotations of individual grains of sand sample under load). However, there are issues when the scale of interest is smaller, for example the characterisation of grain-to-grain contacts (their orientations and evolution) or production of fines by grain breakage. This paper presents a short selection of new grain-scale measurements obtained using existing techniques. The challenges associated with smaller scale measurements on the same images are also discussed through a few examples from ongoing work.