Aus Hydroxamoylchloriden in THF/EtaN bei 20°C [Methode A)] bzw. in siedendem Toluol [Methode B)] in situ erzeugte Nitriloxide oder stabile Nitriloxide im Überschuß in siedendem Toluol [Methode C)] reagieren mit Methylensteroiden unter 1,3‐dipolarer Cycloaddition.
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