In this article, modification of carbon fiber surface by carbon based nanofillers (multi‐walled carbon nanotubes [CNT], carbon nanofibers, and multi‐layered graphene) has been achieved by electrophoretic deposition technique to improve its interfacial bonding with epoxy matrix, with a target to improve the mechanical performance of carbon fiber reinforced polymer composites. Flexural and short beam shear properties of the composites were studied at extreme temperature conditions; in‐situ cryo, room and elevated temperature (−196, 30, and 120°C respectively). Laminate reinforced with CNT grafted carbon fibers exhibited highest delamination resistance with maximum improvement in flexural strength as well as in inter‐laminar shear strength (ILSS) among all the carbon fiber reinforced epoxy (CE) composites at all in‐situ temperatures. CNT modified CE composite showed increment of 9% in flexural strength and 17.43% in ILSS when compared to that of unmodified CE composite at room temperature (30°C). Thermomechanical properties were investigated using dynamic mechanical analysis. Fractography was also carried out to study different modes of failure of the composites.
Carbon fiber reinforced epoxy (CE) composite is ideal for a cryogenic fuel storage tank in space applications due to its unmatched specific strength and modulus. In this article, inter-laminar shear strength (ILSS) of carbon fiber/epoxy (CE) composite is shown to be considerably improved by engineering the interface with carboxyl functionalized multi-walled carbon nanotube (FCNT) using electrophoretic deposition technique. FCNT deposited fibers from different bath concentrations (0.3, 0.5, and 1.0 g/L) were used to fabricate the laminates, which were then tested at room (30 C) and in-situ liquid nitrogen (LN) (À196 C) temperature as well as conditioning for different time durations (0.25, 0.5, 1, 6, and 12 h) followed by immediate RT testing to study the applicability of these engineered materials at the cryogenic environment. A maximum increment in ILSS was noticed at bath concentration of 0.5 g/L, which was $21% and $ 17% higher than neat composite at 30 C and À 196 C, respectively. Short-term LN conditioning was found to be detrimental due to developed cryogenic shock, which was further found to be compensated by cryogenic interfacial clamping upon long-term exposure.
Carbon fibre reinforced polymer (CFRP) composites a perfect structural material due to their outstanding malleable strength, great rigidity, light mass and pronounced thermal resistance. But their inferior out-of-plane properties which are controlled by the matrix–fibre interface restrict the use of CFRP composites in critical applications. Amalgamation of nanofiller in the CFRP composites has found to improve the matrix-fibre interface and there by out-of-plane response. Though matrix modification has contributed to the improvement of interface, fibre modification has a scope for higher levels of nanofiller incorporation and proper fibre nanofiller adhesion. Out of several methods available for fibre modification electrophoretic deposition (EPD) is an eye-catching method for monitoring as well for nanofiller deposition. In recent ages, Graphene has grabbed wonderful consideration Among the graphene based functionalised nanofillers Carboxyl functionalized Graphene (G-COOH) modified CFRP composites have shown better ILSS properties. This research primarily aims to fabricate a CFRP composite using G-COOH modified carbon fibres with varying nanofiller concentrations of 0.5g/ltr, 1g/ltr and 1.5g/ltr in the EPD bath and its impact on the mechanical properties of the FRP composites. The laminates thus obtained were subjected to short beam shear test for the determination of inter laminar shear strength (ILSS). Fractography of the tested samples to observe various failure modes has been carried out by using scanning electron microscope (SEM).
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