A major impediment to the widespread use of asphalt concrete with a high content of reclaimed asphalt pavement (RAP) is uncertainty in the degree of blending between the RAP and the fresh binder. Furthering knowledge concerning the blending between RAP and fresh binder has been difficult because of the lack of an experimental method to quantify the degree of blending in asphalt concrete. This study introduces energy dispersive X-ray spectroscopy (EDS) scanning electron microscopy (SEM) as a means to analyze the degree of blending between RAP and fresh materials in asphalt concrete. EDS allows for mapping the distribution and relative proportion of elements in a sample, hence, allowing for the detection of the distribution of elements in an asphalt concrete specimen. Fresh and RAP binders will have a similar elemental composition. Therefore, titanium dioxide in a fine powder form (0.15-µm particles) is blended with the fresh binder as a tracer before the production of asphalt concrete to enable delineation of the RAP and fresh binders using EDS SEM. The efficacy of EDS SEM for quantifying the degree of blending between RAP and fresh binders in asphalt concrete is demonstrated with two high RAP content mixtures.
The use of small specimen geometries in asphalt mixture performance testing to enable the testing of as-built pavement layers has been gaining attention in recent years. Small specimens could also improve the testing efficiency of laboratory-fabricated specimens by allowing the extraction of multiple test specimens per gyratory-compacted sample. Rigorous assessment of the small specimen geometries is required before the use of such geometries is standardized. In this study, small specimens were evaluated for dynamic modulus and simplified viscoelastic continuum damage fatigue. Three specimen geometries (100-mm- and 38-mm-diameter cylindrical specimens and 25- × 50-mm prismatic specimens) were compared by using five mixtures with a nominal maximum aggregate size (NMAS) ranging from 9.5 to 25.0 mm. The results show that the dynamic modulus and phase angle master curves agreed at low and intermediate temperatures, regardless of the NMAS values of the mixture. At the high temperature, the small specimen dynamic modulus values were slightly higher and the phase angle values were slightly lower than those of the large specimens. The specimen-to-specimen variability for the large and small specimens was comparable. The fatigue test results for the mixtures evaluated were comparable, except for the 25-mm mixture, which proved problematic in the testing of both small and large specimens. Pavement performance was predicted by the layered viscoelastic analysis for critical distresses program by using the test results for the small and large specimens. These results suggest that specimen geometry had a minimal effect on pavement fatigue damage predictions, which indicates promise for the use of small specimen geometries in practice.
Several past studies have demonstrated merit to using tracer‐based energy dispersive X‐ray spectroscopy (EDS) analysis to investigate blending between virgin and recycled materials in asphalt mixtures. However, these past studies have focused on proof of concept and did not establish robust fabrication and microscopy procedures. This study rigorously evaluates the ability to form a stable blend between the tracer and virgin asphalt binder, and the potential for tracer smearing during the preparation of EDS specimens. The results demonstrate that a high shear mixer can be used to prepare homogeneous, stable blends of a titanium dioxide tracer and virgin binder. A critical evaluation of an asphalt mixture specimen prepared to contain specific areas with and without the tracer demonstrates no evidence of tracer smearing due to sample preparation. The results demonstrate that tracer‐based EDS analysis of asphalt mixtures can measure local recycled material availability.
One of the challenges of engineering asphalt mixtures containing reclaimed asphalt pavement (RAP) is uncertainty in the proportion of the total recycled asphalt binder that is available to interact and blend with the virgin asphalt, referred to as the recycled binder availability. The industry presently lacks a practical method to quantify RAP binder availability. Research has shown that the primary source of unavailable recycled binder is agglomerations of adhered RAP particles. The binder bound within the agglomerations is unavailable to contact and therefore blend with virgin asphalt. Building on this knowledge, this study establishes a practical method to quantify the extent of RAP agglomeration and, in turn, RAP binder availability by comparing the gradation of recovered RAP aggregates with that of the RAP itself. A size-exclusion method and corresponding predictive equation to estimate RAP binder availability from the high-temperature performance grade of recovered RAP binder and mixing temperature were also assessed. Four RAP sources were evaluated. Each RAP stockpile was paired with virgin aggregates from the same plant that the RAP was sourced at to produce eight mixtures. Tracer-based microscopy measurements within the eight mixtures were generally in good agreement with the estimations of recycled binder availability using sieve analysis. Implementing the size-exclusion method was challenging with local aggregate, and estimates using the predictive equation yielded in some cases good but overall poorer agreement with the measurements of recycled binder availability from tracer-based microscopy compared with the sieve analysis approach.
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