Attributed to high stability and reproducibility, non-enzymatic electrochemical sensors have been extensively utilized in detection of various chemical substances. In this study, multi-walled carbon nanotube (MWCNT)/Ti-doped ZnO composite was prepared for fabrication of working electrode used in detection of glutamate and ascorbic acid. Ti-doped ZnO particles with the average size of 44.47 ± 4.05 nanometers were synthesized by the solution combustion technique. Hydrothermal impregnation was employed in preparation of the MWCNT/Ti-doped ZnO composite. Electrocatalytic activities of the
Although barium titanate (BaTiO3) shows prominent dielectric properties for fabricating electronic devices, its utilization in electrochemical applications is limited. Thus, this study examined the potential of a BaTiO3-based composite in the detection of a food additive, i.e., citric acid. First, a submicron-scale BaTiO3 powder was synthesized using the solution combustion method. Then, a BaTiO3/multiwalled carbon nanotube (MWCNT) composite was hydrothermally synthesized at BaTiO3:MWCNT mass ratios of 1:1 and 2:1. This composite was used as a working electrode in a nonenzymatic sensor to evaluate its electrocatalytic activity. Cyclic voltammetric measurements revealed that the BaTiO3/MWCNT composite (2:1) exhibited the highest electrocatalytic activity. Reduction reactions were observed at applied voltages of approximately 0.02 and −0.67 V, whereas oxidation reactions were detected at −0.65 and 0.47 V. With acceptable sensitivity, decent selectivity, and fair stability, the BaTiO3/MWCNT composite (2:1) showed good potential for citric acid detection.
The fabrics coated with TiO2 photocatalyst and fluoropolymer exhibit good water-repellent and antimicrobial properties. The coated fabrics can be used in the fabrication of smart gowns and scrub suits as protective clothing for medical staff.
With unique electrical and catalytic properties, CuO has been ubiquitously employed in many applications including electrochemical sensors. Enhanced electrocatalytic performance of CuO can be achieved through doping. This work explored the potential of 3 mol% Fe-doped CuO/multi-walled carbon nanotube (MWCNT) composite for nitrite detection. The undoped CuO and 3 mol% Fe-doped CuO powders, prepared using a solution combustion technique, had average particle sizes lower than 100 nanometres. Particle refinement and enhancement of the specific surface area were observed in 3 mol% Fe-doped CuO. CuO/MWCNT and 3 mol% Fe-doped CuO/MWCNT composites, prepared using the hydrothermal impregnation technique, were tested for their electrocatalytic activities in the presence of nitrite. Cyclic voltammetry results revealed reduction reaction at an applied voltage of approximately −0.4 V. Superior peak currents were evident in the 3 mol% Fe-doped CuO/MWCNT composite. With acceptable sensitivity, limit of detection, selectivity, reusability, and recovery percentage, the 3 mol% Fe-doped CuO/MWCNT composite demonstrated potential capability in the detection of nitrite.
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