Initial displacement estimation is one of the most critical issues in digital image correlation. A better initial value can greatly improve the convergence rate and accuracy of the algorithms with subpixel accuracy. This paper developed an efficient estimation method to yield high-quality initial displacement fields. This method finds the initial displacement of each subset in a prediction-correction way, in which the displacement of the seed point is found by exhaustive search, but the other subsets are first predicted by an extrapolation scheme and then corrected by a monotonous search strategy. This method was tested by extensive experiments and validated by comparing with the well-known exhaustive search and adaptive rood pattern search methods, and then it was combined with the inverse compositional Gauss-Newton algorithm to perform subpixel-optimization experiments. The results demonstrated excellent features of accuracy, effectiveness, and convergence. Finally, we presented a three-dimensional surface reconstruction experiment using the proposed method, obtaining a geometric accuracy with a relative error of 0.016%.
The excellent adsorption and rapid separation capabilities of magnetic MOFs make them desirable pretreatment materials for solid substrates. In this study, magnetic ZIF-8 (mZIF-8) was synthesized in situ by a one-step method in the aqueous solution of magnetic beads. Isothermal adsorption verified that the maximum adsorption capacity of (011) crystal-exposed rhombic dodecahedral ZIF-8 for chloramphenicol was up to 128.31 mg/g (mZIF-8 = 67.18 mg/g). Kinetic adsorption revealed that the type of ZIF-8/mZIF-8 adsorption on chloramphenicol belongs to the pseudo-secondary adsorption kinetics of chemical monomolecular layers. Characterization by FTIR, XPS, and XRD revealed that mZIF-8 interacts with chloramphenicol mainly by π-π electron stacking, electrostatic attraction, and hydrogen bonding interaction. ELISA confirmed that chloramphenicol remained antigenically active after adsorption by mZIF-8. The adsorption and separation of chloramphenicol residues in chicken and egg were completed by mZIF-8 within 20 min. mZIF-8 can be used directly for elution-free ELISA after the adsorption of chloramphenicol. The limits of detection (IC10) of the mZIF-8 + ELISA in chicken and eggs were 1.18 ng/mL and 0.64 ng/mL, respectively. mZIF-8 is expected to be used as a magnetic solid-phase extraction material for the rapid pretreatment of antibiotic residues in other complex solid matrices.
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