Novel styrylquinoline methacrylic monomers and their copolymers with methylmethacrylate (MMA) are presented. The polymerization was carried out in DMF with AIBN as initiator. The products of polymerization were characterized by 1 H NMR. The monomer reactivity ratios for the homogeneous free-radical copolymerization of styrylquinoline monomers and MMA were determined from 1 H NMR spectroscopy data and estimated with the Fineman-Ross (FR) and calculation methods.

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