An environmentally friendly chromium-free insulating coating suitable for oriented silicon steel was prepared by using aluminium dihydrogen phosphate, silica sol, water-based resin, sodium tetraborate and graphene aqueous dispersion as main raw materials. The morphology of the insulating coating was characterized by scanning electron microscopy. Corrosion resistance was investigated by neutral salt spray test and electrochemical test. Magnetic properties and surface insulating resistance were measured. The results showed that the surface of the insulating coating was flat; the addition of graphene could effectively improve the corrosion resistance and magnetic properties of the coating. The corrosion rate in the salt spray test was less than 10% after 120h, and the core loss was reduced by 9.57%. The addition of the graphene did not destroy the insulation properties of the coating. The surface insulation resistance per side of the coating was 269.51 Ω⋅mm2.
Industrial waste has a high potential for reuse in the production of refractories, which can significantly lower costs. The purpose of the research is to access the role of three types of recycled industrial wastes (ferro‐titanium slag [FTS], ferhro‐chromium slag [FCS], and ferro‐vanadium slag [FVS]) utilized as aggregate in the traditional Al2O3‐SiC‐SiO2‐C refractories (ASSC). Erosion and corrosion resistance characterization was performed to determine whether these industrial waste‐containing ASSC still perform better than traditional ASSC during service. Based on the results, incorporating FVS into the ASSC was not recommended, its corrosion resistance was significantly reduced due to the presence of excessive liquid phase. Nonetheless, FTS and FCS could be added as aggregate to the ASSC without affecting their performance. This necessity of the proper amount of liquid phase in ASSC was highlighted in this research since the parameters could alter its properties. Furthermore, the Ti(C,N) transformed from TiO2 in FTS via carbothermal reduction nitridation could effectively prevent further corrosion, and Cr2O3 derived from the decomposition of (Al,Cr)2O3 solid solution in FCS could play the same role during the corrosion process, both of which may be potential raw materials to be used in refractories.
Submicron materials are those with particle size diameters between 0.1 and 1 μm. Submicron SiO2 generally refers to SiO2 powder with a D90 < 1 μm (D90 refers to the particle size distribution exhibited by the sample and corresponds, in this case, to 90% of the particles not exceeding a diameter of 1 μm). In this study, a new type of cement-free iron ditch castable was prepared using dense corundum and silicon carbide as the primary raw materials with submicron SiO2 powder as the binder. The effects of submicron SiO2 powder content on the bulk density, apparent porosity, linear rate of change, compressive strength, and bending strength were investigated. The mechanism of action of the submicron SiO2 powder was also investigated by analyzing its microstructure and particle size distribution. The results revealed that (1) the submicron SiO2 powder can be used as the sole bonding agent in the preparation of cement-free iron ditch castables; (2) in comparison to traditional castables, the cement-free castable developed in this study demonstrated strong service performance and high-temperature bending strength.
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