Bifunctional Fe3O4@Ag
nanoparticles with both superparamagnetic and antibacterial
properties were prepared by reducing silver nitrate on the surface of
Fe3O4
nanoparticles using the water-in-oil microemulsion method. Formation of well-dispersed nanoparticles with
sizes of 60 ± 20 nm was confirmed by transmission electron microscopy and dynamic light scattering.
X-ray diffraction patterns and UV–visible spectroscopy indicated that both
Fe3O4
and silver are present in the same particle. The superparamagnetism of
Fe3O4@Ag
nanoparticles was confirmed with a vibrating sample magnetometer. Their
antibacterial activity was evaluated by means of minimum inhibitory concentration
value, flow cytometry, and antibacterial rate assays. The results showed that
Fe3O4@Ag
nanoparticles presented good antibacterial performance against
Escherichia coli (gram-negative bacteria), Staphylococcus epidermidis
(gram-positive bacteria) and Bacillus subtilis (spore bacteria). Furthermore,
Fe3O4@Ag
nanoparticles can be easily removed from water by using a
magnetic field to avoid contamination of surroundings. Reclaimed
Fe3O4@Ag
nanoparticles can still have antibacterial capability and can be reused.
Polyacrylonitrile/lignin sulfonate (PAN/LS) blend fibers were spun via a wet spinning process. The fiber structure, mechanical properties and thermal stability of the precursor fibers were studied by FT-IR, SEM, tensile tester, and TG-DSC. Results indicated that there was no chemical crosslinking between PAN and LS during the process of wet spinning. PAN and LS had good compatibility in the blend fibers. LS could weaken the skin of the blend fibers and reduce the fiber structure defects. The increase of dope concentration could improve the fiber structure and mechanical properties. LS blending with PAN could reduce fiber weight loss in the thermal stabilization process, and most importantly the precursor fibers could be stabilized rapidly without fiber fusion. Through polymer blending and wet spinning, this study provided a promising way to prepare a precursor fiber for carbon fiber.
A hierarchical microporous carbon material with a Brunauer–Emmett–Teller surface area of 1348 m2 g−1 and a pore volume of 0.67 cm3 g−1 was prepared from yeast through chemical activation with potassium hydroxide. This type of material contains large numbers of nitrogen‐containing groups (nitrogen content >5.3 wt %), and, consequently, basic sites. As a result, this material shows a faster adsorption rate and a higher adsorption capacity of CO2 than the material obtained by directly carbonizing yeast under the same conditions. The difference is more pronounced in the presence of N2 or H2O, showing that chemical activation of discarded yeast with potassium hydroxide could afford high‐performance microporous carbon materials for the capture of CO2.
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