The purpose of this study was to evaluate the effects of the various surface treatment methods on the retention of single crowns on implant abutments. The study included 50 single crowns that were cemented with adhesive resin cement onto the ITI solid abutments. The specimens were randomly divided into 5 groups, each including 10 specimens according to the following surface treatments: group C, control, abutments remained unaltered as control; group L, etching with CO(2) laser; group SB, sandblasting with 50-μm Al(2)O(3); group MS: coating with titanium nitride (TiAlN) with a radiofrequency magnetron sputtering system; and group SP, silicoating by Silano-Pen. After the surface treatment procedures were finished, the casted crowns were cemented onto the abutments, and thermocycling was applied to simulate oral environment. The uniaxial tensile force was applied to all test crowns using a universal test machine (Instron) with a crosshead speed of 0.5 mm/min. The load required to dislodge each crown was recorded in Newton. The lowest tensile bond strength values were obtained with group MS (223.26 ± 14.30 N) and significantly differ from all other groups except group C. Group SB showed highest test results (506.02 ± 18.04 N) and differs from other groups (P < .05). The test values that were obtained in group MS-group C did not show significant differences (P > .05). Sandblasting is an effective method to increase bond strength. Also, Silano-Pen and laser application is advisable for increasing the crown retention to abutments. Titanium aluminum nitride coating with magnetron sputtering technique seems to be ineffective.
PURPOSEAlthough several surface treatments have been recently investigated both under in vitro and in vivo conditions, controversy still exists regarding the selection of the most appropriate zirconia surface pre-treatment. The purpose of this study was to evaluate the effect of alumina (Al) and aluminium nitride (AlN) coating on the shear bond strength of adhesive resin cement to zirconia core.MATERIALS AND METHODSFifty zirconia core discs were divided into 5 groups; air particle abrasion with 50 µm aluminum oxide particles (Al2O3), polishing + Al coating, polishing + AlN coating, air particle abrasion with 50 µm Al2O3 + Al coating and air particle abrasion with 50 µm Al2O3 + AlN coating. Composite resin discs were cemented to each of specimens. Shear bond strength (MPa) was measured using a universal testing machine. The effects of the surface preparations on each specimen were examined with scanning electron microscope (SEM). Data were statistically analyzed by one-way ANOVA (α=.05).RESULTSThe highest bond strengths were obtained by air abrasion with 50 µm Al2O3, the lowest bond strengths were obtained in polishing + Al coating group (P<.05).CONCLUSIONAl and AlN coatings using the reactive magnetron sputtering technique were found to be ineffective to increase the bond strength of adhesive resin cement to zirconia core.
Titanium-based alloys have gained worldwide application over the past century. However, their low wear resistance remains an unresolved challenge for the Ti6Al4V alloy, which has significant industrial use. Therefore, it is an integral part in material selection and surface treatment in friction-wear applications. Tribological properties are not only material parameters but also system parameters where test conditions are essential. Hardness, roughness and contact conditions of coatings, which are especially important in surface treatments, affect wear modes. In this study, titanium nitride, titanium aluminum nitride and titanium carbon nitride coatings were obtained by unbalanced reactive magnetron sputtering to improve the weak tribological properties of Ti6Al4V alloy. The wear behavior was studied at room temperature in dry conditions. Wear tests were conducted under different loads and different sliding rates, which were followed by comparative analyses of their wear resistances. While the coated samples showed higher wear resistance than the uncoated Ti6Al4V alloy, the lowest wear track width was observed in TiN coating. Depending on the surface properties of the coatings, adhesion, abrasion and oxidation wear mechanisms were observed. It was concluded that a TiN coating could be a material of choice for applications where triple abrasive wear is dominant.
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