This work presents the results of obtaining the sulfur nanoparticles, which can be used in agriculture as a fungicide. Sulfur nanoparticles were obtained by modifying the surface of sulfur using various surfactants including cetyltriammoniumbromide (CTAB), sodium dodecylbenzene sulfanate (SDBS) and Triton X-100 (TX-100). The size, crystal structure and morphology of sulfur nanoparticles were determined by methods as laser size analyzing (LSA), X-ray diffraction (XRD), scanning electron microscope (SEM). It was found that the nanoparticles had a sulfur monoclinic β-form struture, and their average size was in the range of 1000-1500 nm.
Sulfur is a nonmetallic element necessary for life. Sulfur nanopartieles display unique physical and chemical feature because of effects such as the quantum size effect, mini size effect, surface effect and macro-quantum tunnel effect. So sulfur nanoparticles would present higher efficacies such as removal of heavy metals, radical-scavenging, antimicrobial activity, antioxidant and antitumor activities. It is used as a fungicide product in agriculture, also used in medicine, to obtain sulfur fertilizers and cosmetics industries, as well as in obtaining nanocomposite lithium batteries. In synthesis of sulfur nanowires with carbon to from hybrid materials with useful properties for gas sensor and catalytic applications. This work presents the results of obtaining the sulfur nanoparticles, which can be used in agriculture as a fungicide treatment. Sulfur nanoparticles were obtained by modifying the surface of sulfur by various surfactants including cetyltriammoniumbromide (CTABr), Sulfanol, Sodium Ligninsulfonate (CMN), Sodium salt of polynaphthalene sulphonic acid (NNO), water soluble polymer sodium carboxymethylcellulose (NaCMC), mineral mixtures and their compositions. The size and the structure of sulfur nanoparticles were determined by methods as LSA, XRD, SEM. Been studied the value of adsorption at the interface of solid/gas. It is shown that the nanoparticles have a sulfur monoclinic B-form, and their average size is in the range 500-1000 nm. The received products can be considered as perspective forms of application in agriculture.
Sulfur nanoparticles display unique physical and chemical feature because of effects such as the quantum size effect, mini size effect, surface effect, and macro-quantum tunnel effect. Therefore, sulfur nanoparticles would present higher efficacies such as removal of heavy metals, radical-scavenging, antimicrobial activity, antioxidant and antitumor activities. They have been using as a fungicide product in agriculture and medicine; to obtain sulfur fertilizers and cosmetics industries, as well as in obtaining nanocomposite lithium batteries; to form stable carbon chains such as C 3 S and C 5 S for obtaining hybrid materials with useful properties for gas sensor and catalytic applications. This work presents the results of obtaining sulfur nanoparticles, which can be used in agriculture as a fungicide treatment. Sulfur nanoparticles were obtained by modifying the surface of sulfur by various water-soluble polyelectrolyte (WSP)/surfactant mixtures including NaCMC/CTAB, PDADMAC/SDBS, NaCMC/Triton X-100 (TX-100). The size and the structure of sulfur nanoparticles were determined by methods as LSA, XRD, SEM. It is shown that the nanoparticles have a sulfur monoclinic α-form, and their average size is in the range of 100-300 nm. The received products can be considered as perspective forms of application in agriculture and medicine.
Heat-resistant concrete with liquid and water glassis widely used for the lining of thermal units and equipment. In this paper we present the results of studies on the preparation and study of the properties of the sodium silicate composite binder (SNCR) on the basis of quartzite Kulantyubinsky field for heat-resistant concrete. Refractoriness quartzite 1450-1500 ° C. According to RFA quartzite consists of α - quartz, in addition, the sample contains kaolinite Al2O3 ∙ 2SiO2 ∙ H2O. SNCR is prepared jointly grinding quartzite and solid sodium silicate, a ball mill, taken from ootnoshenii: 90:10, 85:15, 80:20 to surface area 2800-3000 cm 2/g. To determine the optimal composition of the binder were determined flexural and compressive strength of samples, cross members 16х4х4 see Hardening SNCR carried drying in 2-stage operation in the temperature range 100-200 оC. Found that the bending strength of SNCR is 1.6-2.6 MPa, compressive 17,0-32,3 MPa.Refractoriness of 1320-1390 °C. The process of phase formation during heat treatment optimum binder composition.Was found that at temperatures of 1200-1300 ° C in SNCR by quartzite than β - quartz formed vykotemperaturnaya modification quartz β - cristobalite, which increases the fire resistance of binder. Presence of cristobalite phase was also found with the mineralogical On-petrographic method as well. resulting binder can be used for acid-and heat-resistant refractory Producth with 1300 оC and more.
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