35 Cl NQR and XRD have been investigated on the solid solution Cs 2 [Ag(I) x Au(I) 1−x Cl 2 ][Au(III)Cl 4 ] which yielded NQR lines by annealing. The crystal forms a tetragonal cell in the whole range of x. However, a change of the modification occurs at x ≈ 0.85. The increase of c and decrease of a were observed in the range of 0.0 ≤ x ≤ 0.7.
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